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← Document results/DEP Box 18/GCMS X 5/10/02 A 5/14/02
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GCMS calibration verification for sample AE10901, May 2002

Machine-extracted title · confidence 95%

Calibration data for volatile organic compounds including nitrobenzene and isophorone from sample AE10901 analysis.

NYC-WTC_000023863–000023870

Folder label: “GCMS X 5/10/02 A 5/14/02

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NYC 9/11 Public Portal Document QUCIILALCLLOIi RSDOL L 11 IC V LCwcu)

Data File : C:\MSDCHEM\1\DATA\051402\510REF1.D Vial: 4 Acq On : 14 May 2002 3:56 pm Operator: Mclean Sample : 5/10 kb Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 16 14:43:01 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title :508 Modified GC/MS scan Last Update : Thu May 16 14:34:28 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.54 202 8580138 18.66 ug/L 99 3 8) Pyrene 27.17 202 8987367 20.61 ug/L 98 39) Butylbenzylphthalate 29.53 149 2650508 13.64 ug/L # 96 40) Benzo(a)anthracene 30.79 228 6047256 17.42 ug/L 97 41) Bis(2-ethylhexyl)phthalate 31.39 149 3124580 11.90 ug/L 95 42) Chrysene 30.88 228 6811359m 18.95 ug/L 44) Di-n-octylphthalate 33.24 149 2646005 8.53 ug/L # 97 45) Benzo(b)fluoranthene 33.75 252 4407538 17.32 ug/L 97 46) Benzo(k)fluoranthene 33.83 252 6969392 21.79 ug/L 99 47) Benzo(a)pyrene 34.55 252 3225900m 12.70 ug/L 48) Indeno(1,2,3-cd)pyrene 37.39 276 1688660 9.48 ug/L 98 49) Dibenz(a,h)anthracene 37.51 278 2477281 13.08 ug/L 99 50) Benzo(g,h,i)perylene 38.14 276 3551073 17.86 ug/L 98

(#) = qualifier out of range (m) = manual integration (+) = signals summed 510REF1.D 050102.M Thu May 16 14:43:38 2002 Page 2

NYC-WTC_000023866

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NYC-WTC_000023866Source: NYC Law Department, mirrored locally

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