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GCMS quantitative results for sample AE11602, May 2002

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GCMS calculation report for sample AE11602 dated May 30, 2002, listing concentrations of nitrosamines and chlorinated compounds.

NYC-WTC_000013913–000013920

Folder label: “GCMS X 5/24/02 A 5/28/02

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NYC 9/11 Public Portal Document UCtLLGt.Ol RCDOL L LL acvcwc)

Data File : C:\MSDCHEM\1\DATA\052802\524REF2.D Vial: 5 Acq On : 28 May 2002 5:34 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 30 10:36:24 2002 Quant Results File: 052202.RES Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed May 29 08:47:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoroanthene 26.49 202 6519955 15.36 ug/L 98 38) Pyrene 27.13 202 6721049 21.64 ug/L 99 39) Butylbenzylphthalate 29.48 149 1509916 11.36 ug/L 97 40) Benzo(a)anthracene 30.73 228 3815512 16.27 ug/L 99 41) Bis(2-ethylhexyl)phthalate 31.34 149 1330126 7.69 ug/L 96 42) Chrysene 30.82 228 4536135m 16.84 ug/L 44) Di-n-octylphthalate 33.18 149 908263 5.47 ug/L # 94 45) Benzo(b)fluoranthene 33.70 252 2451411 16.04 ug/L 99 46) Benzo(k)fluoranthene 33.77 252 3400765 19.87 ug/L 99 47) Benzo(a)pyrene 34.50 252 1436949 10.51 ug/L 99 48) Indeno(l,2,3-cd)pyrene 37.32 276 752915 8.26 ug/L 93 49) Dibenz(a,h)anthracene 37.44 278 1170241 11.68 ug/L 99 50) Benzo(g,h,i)perylene 38.05 276 1496558 14.06 ug/L 97

(#) = qualifier out of range (m) = manual integration (+) = signals summed 524REF2.D 052202.M Thu May 30 10:36:48 2002 Page 2

NYC-WTC_000013918

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NYC-WTC_000013918Source: NYC Law Department, mirrored locally

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