GCMS quantitative results for sample AE11602, May 2002

NYC 9/11 Public Portal Document *MOL 111 IC V LCwCU/

Data File : C:\MSDCHEM\1\DATA\052802\524REF2.D Vial: 5 Acq On : 28 May 2002 5:34 pm Operator: McLean Sample : 5/24 ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 30 10:36:24 2002 Quant Results File: 052202.RES Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed May 29 08:47:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 9.90 152 3979726 40.00 ug/L 0.00 10) Napthalene-d8 13.39 136 16262201 40.00 ug/L -0.02 17) Acenapthalene-dlO 18.53 164 9006857 40.00 ug/L -0.01 29) Phenanthranene-dlO 22.91 188 13434563 40.00 ug/L -0.01 37) Chrysene-dl2 30.76 240 7821105 40.00 ug/L -0.05 43) Perylene-dl2 34.65 264 3847802 40.00 ug/L -0.03 System Monitoring Compounds 27) TCMX 20.50 209 2020011 38.92 ug/L 0.00 Spiked Amount 40.000 Recovery 97.30% Target Compounds Qvalue 2) n-nitros-dimethyl amine 3.90 74 431979 5.82 ug/L # 58 3) bis(2-Chloroethyl)ether 9.31 93 2341048 15.88 ug/L 99 4) 1,3-Dichlorobenzene 9.73 146 2116784 14.25 ug/L 99 5) 1,4-Dichlorobenzene 9.94 146 2254780 13.97 ug/L 99 6) 1,2-Dichlorobenzene 10.32 146 2178886 15.34 ug/1 98 7) 2,2'oxybi s(1-Chioropropane 10.77 45 3806777m 16.85 ug/L 8) N-nitroso-di-propylamine 11.10 70 1599679 16.67 ug/L 98 9) Hexachloroethane 11.22 117 673695 11.52 ug/L 98 11) Nitrobenzene 11.45 77 2247281 15.74 ug/L 98 12) 1sophorone 12.17 82 4807122 18.59 ug/L 100 13) bis(2-Chloroethoxy) methan 12.90 93 2925320 16.14 ug/L 98 14) 1,2,4-Trichiorobenzene 13.26 180 1854321 15.09 ug/L 100 15) Napthalene 13.45 128 7524693 17.55 ug/L 100 16) Hexachlorobutadiene 13.89 225 761056 12.98 ug/L 98 18) 2-Chloronaphthalene 16.89 162 4315192 18.70 ug/L 99 19) Dimethylphthalate 17.96 163 4838444 17.09 ug/L 99 20) 2,6-Dinitrotoluene 18.07 165 775226 17.05 ug/L 99 21) Acenapthylene 18.08 152 6519414 16.94 ug/L 99 22) Acenapthalene 18.62 153 4426288 18.22 ug/L 98 23) 2,4-Dinitrotoluene 19.23 165 1013161 17.04 ug/L 95 24) Diethylphthalate 20.10 149 4821802 18.23 ug/L 97 25) 4-Chlorophenyl-phenylether 20.29 204 2424133 17.17 ug/L 97 26). Fluorene 20.16 166 5305651 18.53 ug/L 99 28) Azobenzene 20.74 77 5281355 16.95 ug/L 98 30) Nnitrosodiphenylamine 20.65 169 2867719 21.15 ug/L 99 31) 4-Bromophenyl-phenylether 21.72 248 1195883 17.38 ug/L 95 32) Hexachlorobenzene 21.75 284 1223376 18.29 ug/L 97 3 3) Phenanthrene 22.97 178 7278209 18.01 ug/L 99 3 4) Anthracene 23.12 178 6557370 16.48 ug/L 99 35) Di-n-butylphthalate 25.05 149 6807583 16.96 ug/L 99 (#) = qualifier out of range (m) = manual integration 524REF2.D 052202.M Thu May 30 10:36:47 2002 Page 1

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