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← Document results/DEP Box 25/GCMS X 5/7/02 A 5/15/02
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GCMS calibration results for sample AE10809, May 2002

Machine-extracted title · confidence 50%

Gas chromatography-mass spectrometry calibration report for sample AE10809 showing measured values for semivolatile organic compounds.

NYC-WTC_000045964–000045967

Folder label: “GCMS X 5/7/02 A 5/15/02

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NYC 9/11 Public Portal Document Data File C:\MSDCHEM\1\DATA\0514 0 2\CAL2 0.D Vial: 15 Acq On 15 May 2002 1:44 am Operator: Mclean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 16 14:20:06 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu May 16 12:34:41 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.54 202 15666526 22.88 ug/L 99 38) Pyrene 27.18 202 14943839 21.10 ug/L 99 39) Butylbenzylphthalate 29.52 149 6612336 20.95 ug/L # 96 40) Benzo(a)anthracene 30.79 228 10932362 19.39 ug/L 97 41) Bis(2-ethylhexyl)phthalate 31.39 149 8648925 20.28 ug/L 97 42) Chrysene 30.89 228 11918624 20.41 ug/L 98 44) Di-n-octylphthalate 33.24 149 11891141 19.97 ug/L 98 45) Benzo(b)fluoranthene 33.75 252 11284964 23.11 ug/L 97 46) Benzo(k)fluoranthene 33.83 252 13393165 21.83 ug/L 99 47) Benzo(a)pyrene 34.56 252 10534759 21.62 ug/L 99 48) Indeno(1,2,3-cd)pyrene 37.39 276 7495984 21.94 ug/L 98 49) Dibenz(a,h)anthracene 37.51 278 7946701 21.87 ug/L 100 50) Benzo(g,h,i)perylene 38.14 276 9005747 23.61 ug/L 98

(#) = qualifier out of range (m) = manual integration (+) = signals summed CAL20.D 050102.M Fri May 17 10:26:41 2002 Page 2

NYC-WTC_000045966

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NYC-WTC_000045966Source: NYC Law Department, mirrored locally

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