GCMS calibration verification for sample AE10901, May 2002

Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\l\DATA\051402\510REFl.D Vial: 4 Acq On : 14 May 2002 3:56 pm Operator: Melean Sample : 5/10 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 16 14:43 2002 Quant Results File: 050102.RES Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu May 16 14:34:28 2002 Response via : Initial Calibration Abundance TIC:51OREF1.D 2600000 86 o

2400000 o o I a g £ 2 Io €s 2200000 l I J: ! 2 z N a

I 2000000

1800000 I 8€ i | % 1600000 | 1 2 3 At Ci 8 a 2 1400000 t 6 8 g C

s I8 I 8 2 Eg 8 i 6 i i& i 1200000 sh | 2 sa § fl 5 2' i23 s a

1000000 Jisllt & 85 288 84 5 s§ 22 I i I Io 5 I fe 9 t = Loe 95 a8 84923 Eo c 2 £ I I1 1 I t. 800000 s 2 8 x s2 2 2 o 58 C 600000 2 § s 8s- 82 to 5 s m 8 1 & a l& g 6 1C J8 N & a $8 I f CD E 400000 J O o l I8 1 Q 200000 ! 5 C

co co co t co o CXI Q 0 — TT ------- ‘1 i 1 — --- ‘I‘I| 11—" 11 j o o o Time-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 o o o 1 Q o 510REF1.D 050102.M Thu May 16 14:43:40 2002 Page 3 — oo sd > > 2 7