Laboratory report of GCMS analysis for sample AE10064 conducted on May 23, 2002, showing surrogate recovery data.
NYC-WTC_000023718–000023727Folder label: “GCMS X 5/9/02 A 5/20/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\MAY0302\10064.D Vial: 37 Acq On 5 May 2002 3:18 am Operator: Sample GC/MS SCAN 4/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 11:57 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table ' Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.19 152 475863 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 1737217 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.13 164 935025 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.58 188 1290497 40.00 ug/1 -0.01 38) Chrysene-dl2 33.63 240 827689 40.00 ug/1 -0.03 44) Perylene-dl2 37.86 264 526235 40.00 ug/1 -0.02 System Monitoring Compounds 28) TCMX 23.27 209 25226 5.54 ug/L -0.02 Spiked Amount 10.000 Recovery = 55.40% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-ChlOroethyl)ether 11.60 93 261 N.D. 4) 1,3-Dichlorobenzene 12.24 146 185 N.D. 5) 1,4-Dichlorobenzene 12.24 146 185 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 14.20 77 372 N.D. 12) 1sophorone 14.53 82 3133 N.D. 13) bis(2-Chloroethoxy)methane 15.21 93 1185 N.D. 14) 1,2,4-Trichlorobenzene 15'71 180 477 N.D. 15) Naphthalene 15.88 128 1869 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 19.39 162 1577 N.D. 20) Dimethylphthalate 20.48 163 4549 N.D. 21) 2,6-Dinitrotoluene 20.70 165 421 N.D. 22) Acenaphthylene 20.66 152 1943 N.D. 2 3) Acenaphthene 21.23 153 2020 N.D. 24) 2,4-Dinitrotoluene 21.88 165 634 N.D. 25) Diethylphthalate 22.61 149 10872 0.46 ug/1 96 26) 4-Chlorophenyl-phenylether 22.77 204 2014 N.D. 27) Fluorene 22.75 166 3596 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. d 32) 4-Bromophenyl-phenylether 24.24 248 1261 N.D. 33) Hexachlorobenzene 24.67 284 1343 N.D. 34) Phenanthrene 0.00 178 0 N.D. d (#) = qualifier out of range (m) = manual integration 10064.D GCMS0501.M Tue May 07 11:57:56 2002 Page 1
NYC-WTC_000023718
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NYC-WTC_000025533
Fragmented GCMS scan data page showing tentative identification of compounds and surrogate recovery for sample AE10812.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022953
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022930
GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023195
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013117
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045452
Technical document displaying GCMS calibration data and compound retention times for sample AE09391 processed in early May 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045507
Technical document displaying GCMS calibration data and compound retention times for sample AE09449 processed in early May 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046294
Laboratory report showing GCMS calibration data for sample AE09585 generated on May 4-6, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046332
Laboratory report showing GCMS calibration data for sample AE09587 generated on May 4-6, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013146
Calibration table listing response factors for deuterated standards and target compounds used in gas chromatography-mass spectrometry analysis.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046351
Laboratory report showing GCMS calibration data for sample AE09334 generated on April 25-26, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011494
Instrument output displaying calibration data and surrogate recovery results for sample AE03381.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000023646
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
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NYC-WTC_000023647
Technical data file header page from a GCMS analysis run associated with the World Trade Center site in May 2002.
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NYC-WTC_000023649
Laboratory report showing GC/MS blank analysis for sample AE09676 with non-detect results for volatile organic compounds.
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NYC-WTC_000023662
Laboratory report showing GC/MS calibration data for volatile organic compounds analyzed on May 20-21, 2002.
Filed in the same folder
NYC-WTC_000023666
Laboratory report showing GC/MS reference analysis for sample AE09676 with quantitative results for volatile organic compounds.
Filed in the same folder