GCMS analysis report for sample AE09523, May 2002

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GCMS results for sample AE09523 showing surrogate recovery and unknown compounds dated May 6, 2002.

NYC-WTC_000043320–000043328

Folder label: “GCMS X 4/22/02 A 5/3/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0202\9523.D Vial: 21 Acq On 3 May 2002 10:38 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 3 12:21 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.20 152 381449 40.00 ug/1 -0.02 10) Naphthalene-d8 15.83 136 1393797 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.14 164 750812 40.00 ug/1 0.00 30) Phenanthrene-diO 25.58 188 1044922 40.00 ug/1 0.00 38) Chrysene-dl2 33.64 240 660892 40.00 ug/1 -0.03 44) Perylene-dl2 37.87 264 424898 40.00 ug/1 0.00

System Monitoring Compounds 28) TCMX 23.27 209 27442- 7.51 ug/L -0.02 Spiked Amount 10.000 Recovery = 75.10%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 11.61 93 394 N.D. 4) 1,3-Dichlorobenzene 12.24 146 178 N.D. 5) 1,4-Dichlorobenzene 12.24 146 178 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 NJ. 11) Nitrobenzene 13.43 77 503 N.D. 12) Isophorone 14.53 82 9901 0.40 g/i # 94 13) bis(2-Chloroethoxy)methane 15.21 93 718 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.89 128 1154 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 19.41 162 423 N.D. 20) Dimethylphthalate 20.48 163 648 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 20.67 152 979 N.D. 23) Acenaphthene 21.23 153 1223 N.D. 24) 2,4-Dinitrotoluene 21.87 165 311 N.D. 25) Diethylphthalate 22.62 149 3814 N.D. 26) 4-Chlorophenyl-phenylether 22.77 204 1362 N.D. 27) Fluorene 22.75 166 2912 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.17 168 914 N.D. 32) 4-Bromophenyl-phenylether 24.24 248 1066 N.D. 33) Hexachlorobenzene 0 : 00 284 0 N.D. d 34) Phenanthrene 0.00 178 0 N.D. d

(#) = qualifier out of range (m) = manual integration 9523.D GCMS0501.M Fri May 03 12:22:03 2002 Page 1

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