NYC-WTC_000023171
Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
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GCMS calibration data for TCLP analysis, May 2002
Machine-extracted title · confidence 90%Calibration table listing response factors for deuterated standards used in TCLP analysis on May 5, 2002.
NYC-WTC_000023148–000023155Folder label: “GCMS X 5/8/02 A 5/9/02”
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NYC 9/11 Public Portal Document
Data File C:\HPCHEM\1\DATA\MAY0 302\9575.D Vial: 48 Acq On 5 May 2002 2:04 pm Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 14:55 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501
Internal Standards R.T. QIon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.19 152 461381 40.00 ug/1 -0.02 10) Naphthalene-d8 15.82 136 1684268 40.00 ug/1 -0.03 17) Acenaphthene-diO 21.14 164 907550 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.57 188 1262110 40.00 ug/1 -0.02 38) Chrysene-dl2 33.64 240 819585 40.00 ug/1 -0.03 44) Perylene-dl2 37.87 264 561502 40.00 ug/1 -0.01 System Monitoring Compounds 28) TCMX 23.27 209 28639 6.48 ug/L -0.02 Spiked Amount 10.000 Recovery = 64.80% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 n.d; 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.88 128 101 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.61 149 961 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.58 178 338 N.D. (#) = qualifier out of range (m) = manual integration 9575.D GCMS0501.M Tue May 07 14:55:38 2002 Page 1
NYC-WTC_000023148
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