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GCMS calibration data for TCLP method, May 2002

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GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

NYC-WTC_000023055–000023062

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C:\HPCHEM\l\DATA\MAY0302\9570.D Vial: 44 Acq On 5 May 2002 10:09 am Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 14:49 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.64 178 2336 N.D. 36) Di-n-butylphthalate 27.55 149 3192 N.D. 37) Fluoranthene 29.26 202 1770 N.D. 3 9) Pyrene 29.94 202 1465 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.63 228 4212 N.D. 42) Bis(2-ethylhexyl)phthalate 33.85 149 2662 N.D. 43) Chrysene 0.00 228 0 N.D. d 45) Di-n-Octylphthalate 35.59 149 1304 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. d 47) Benzo(k)fluoranthene 0.00 252 0 N.D. d 48) Benzo(a)pyrene 37.68 252 775 N.D. 49) Indeno(1,2,3-cd)pyrene 41.95 276 714 N.D. 5 0) Dibenz(a,h)anthracene 42.00 278 266 N.D. 51) Benzo(g,h,i)perylene 43.19 276 713 N.D.

(#) = qualifier out of range (m) = manual integration 9570.D GCMS0501.M Tue May 07 14:50:31 2002 Page 2

NYC-WTC_000023056

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NYC-WTC_000023056Source: NYC Law Department, mirrored locally

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