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GCMS analysis report for sample AE09452, May 2002

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GCMS results for sample AE09452 showing surrogate recovery and unknown compounds dated May 6, 2002.

NYC-WTC_000043273–000043281

Folder label: “GCMS X 4/22/02 A 5/3/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0202\9452.D Vial : 17 Acq On 3 May 2002 6:38 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 3 9:57 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.58 178 324 N.D. 36) Di-n-butylphthalate 27.55 149 6863 N.D. 37) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.65 228 1489 N.D. 42) Bis (2-ethylhexyl)phthalate 33.87 149 8897 0.54 ug/1 # 93 43) Chrysene 33.71 228 495 N.D. 45) Di-n-Octylphthalate 35.60 149 177 N.D. 46) Benzo(b)fluoranthene 36.70 252 104 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.87 252 1558 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 9452.D GCMS0501.M Fri May 03 09:58:35 2002 Page 2

NYC-WTC_000043276

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NYC-WTC_000043276Source: NYC Law Department, mirrored locally

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