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GCMS calibration data for TCLP method, May 2002

Machine-extracted title · confidence 100%

GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

NYC-WTC_000023006–000023013

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0302\LBC.D Vial: 39 . Acq On 5 May 2002 5:15 am Operator: Sample GC/MS SCAN 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.153 337 340 367 rBV 395490 936898 23.22% 4.558% 2 12.194 775 781 797 rBV 1261561 2899124 71.85% 14.104% 3 14.796 1059 1065 1071 rBV 245463 478104 11.85% 2.326% 4 15.823 1171 1177 1191 rBV 1775492 3664664 90.83% 17.829% 5 21.138 1750 1757 1771 rBV 1844432 4034727 100.00% 19.629% 6 23.273 1980 1990 1996 rVB 106688 219729 5.45% 1.069% 7 25.573 2235 2241 2253 rBV2 1697289 3697916 91.65% 17.990% 8 33.637 3114 3121 3136 rBV 1172093 2607780 64.63% 12.687% 9 37.861 3574 3582 3598 rBV2 696032 2015991 49.97% 9.808%

Sum of corrected areas: 20554933 LBC.D GCMS0501.M Tue May 07 15:03:29 2002

NYC-WTC_000023009

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NYC-WTC_000023009Source: NYC Law Department, mirrored locally

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