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GCMS blank analysis results for volatile organics, May 2002

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Laboratory report of gas chromatography mass spectrometry blank analysis for volatile organic compounds conducted on May 9, 2002.

NYC-WTC_000023207–000023215

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0 90 2\LB.D Vial: 3 , Acq On 9 May 2002 4:15 pm Operator: Sample GC/MS SCAN 5/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title :’ 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.159 336 340 371 rBV 708646 1549587 40.12% 7.376% 2 12.191 774 780 798 rBV 1245760 2761357 71.49% 13.143% 3 14.793 1058 1064 1069 rBV 63078 121949 3.16% 0.580% 4 15.829 1170 1177 1194 rBV 1747224 3511881 90.92% 16.716% 5 21.135 1749 1756 1769 rBV 1857251 3862794 100.00% 18.386% 6 23.279 1981 1990 1995 rBV 739529 1516873 39.27% 7.220% 7 25.579 2234 2241 2251 rBV2 1677192 3579464 92.67% 17.037% 8 33.634 3113 3120 3140 rBV2 1042951 2413369 62.48% 11.487% 9 37.867 3573 3582 3601 rBV2 564546 1692282 43.81% 8.055%

Sum of corrected areas: 21009556 LB.D GCMS0510.M Fri May 10 13:59:29 2002

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NYC-WTC_000023211Source: NYC Law Department, mirrored locally

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