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GCMS analysis results, sample AE09151, May 2002

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GCMS analytical report for environmental sample AE09151 including surrogate compound data from May 15, 2002.

NYC-WTC_000022795–000022811

Folder label: “GCMS X 5/8/02 A 5/10/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\050902\9151.D Vial: 18 Acq On : 10 May 2002 5:58 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 1-Docosene Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.00 0.78 ug/L 951132 Chrysene-dl2 30.81

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Docosene 308 C22H44 001599-67-3 68 2 1-Heptadecanol 256 C17H360 001454-85-9 64 3 Dodecyl acrylate 240 C15H28O2 002156-97-0 64 4 2-Propenoic acid, n-pentadecyl e... 282 C18H3402 1000245-64-0 64 Abundance Scan 4412 (29.002 min): 9151 .D (-4404) (-) m/ z 55.10 100.00% 55

5000 69 83 97 4 / PTTTt Ad . 111 127 28.60 28.80 29.00 29.20 29.40 11 ,ll 141 ■n/z-> O+ TTT 20 40 4 Ir ill! nil ........................................................................ 1'"1 I 11''I'1’11'1''11‘'I 111'I‘'1 1 ' ''1 1 60 80 100 120 140 160 180 200 220 240 260 280 300 i' ■' ‘ i m/z 43.10 51.81% Abundance #111438:1 -Docosene 4' 5$ 69 83 97 M MMWN 5000 AA—AA—4—44 28.60 28.80 29.00 29.20 29.40 111 m/z 57.10 49.08% 2" 125

n/z-> 0! "’IT 20 440+— 60 80 100 120I 139153167181 11 140 160 180 200 220 240 260 280 300 11 1 "111 Mi 11II f 1111111111 mPTI । । ■ 11111111 308

Abundance #13564:1-Heptadecanol

4 55 69 83 97 1 MA .A... L 28.60 28.80 29.00 29.20 29.40 5000 m/ z 69.10 45.30% 111 125 271 J .I l 139 154168182 210 238 4 0+ T-I-T-f 4— TT M .. M ..................................................................................................................................................... ■.......................... i'''' i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #111268: Dodecyl acrylate 55 28.60 28.80 29.00 29.20 29.40 m/ z 83.10 44.67%

5000 41 73 127 0 ■' i ■ ■ ■ ■ i + 1 । WI i |4i1, 1h97 i 111 1, । -A i r 168 I ■ ■ ■' i11 ■' i'1 ■11 ■ ■1 ■ i' ■' ■ i ■ ■ ■ ■ i' ■ ■' i' ‘ ' i' ■ i ■ ■ ■ ■ i ■ ■ 44 . m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 28.60 28.80 29.00 29.20 29.40

9151.D 050102.M Mon May 13 11:28:06 2002 Page 9

NYC-WTC_000022810

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NYC-WTC_000022810Source: NYC Law Department, mirrored locally

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