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← Document results/DEP Box 18/GCMS X 5/8/02 A 5/10/02
Document / 7 pages

GCMS calibration table review, April 2002

Machine-extracted title · confidence 100%

Reviewed data file listing retention times and response factors for deuterated internal standards.

NYC-WTC_000022788–000022794

Folder label: “GCMS X 5/8/02 A 5/10/02

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Scanned page image, NYC-WTC_000022791
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\MAY0 3 02\9331.D Vial: 33 Acq On 4 May 2002 11:23 pm Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.162 337 341 346 rBV 452251 890884 23.70% 4.627% 2 12.194 775 781 796 rVB 1173860 2719886 72.35% 14.126% 3 15.823 1171 1177 1193 rBV 1636097 3440441 91.52% 17.869% 4 21.138 1750 1757 1771 rBV 1729813 3759120 100.00% 19.524% 5 23.273 1981 1990 1998 rVB 111785 220581 5.87% 1.146%

6 25.573 2234 2241 2252 rBV2 1581399 3490632 92.86% 18.129% 7 33.637 3114 3121 3137 rBV2 1109258 2480480 65.99% 12.883% 8 33.857 3140 3145 3160 rVB 160926 368147 9.79% 1.912% 9 37.862 3574 3582 3601 rBV2 638148 1883961 50.12% 9.785%

Sum of corrected areas: 19254132

9331.D GCMS0501.M Tue May 07 12:01:36 2002

NYC-WTC_000022791

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NYC-WTC_000022791Source: NYC Law Department, mirrored locally

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