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GCMS analysis results for sample AE09447, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE09447 including surrogate recovery data conducted on May 15, 2002.

NYC-WTC_000045462–000045471

Folder label: “GCMS X 5/3/02 A 5/8/02

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Scanned page image, NYC-WTC_000045467
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C : \HPCHEM\ 1 \DATA\MAY0 8 0 2 \ 94 4 7 . D Vial: 12 Acq On 8 May 2002 9:20 pm Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.162 337 341 371 rVB 376811 916194 26.84% 4.908% 2 12.194 775 781 796 rVB 1027184 2437997 71.43% 13.059% 3 15.823 1171 1177 1195 rBV 1480540 3082455 90.31% 16.511% 4 21.129 1750 1756 1777 rBV 1626814 3413041 100.00% 18.282% 5 23.273 1981 1990 2001 rBV2 157164 341280 10.00% 1.828%

6 25.573 2235 2241 2252 rW2 1422044 3040581 89.09% 16.287% 7 33.628 3114 3120 3136 rBV2 773553 1819166 53.30% 9.745% 8 36.130 3385 3393 3421 rBV 857012 2320621 67.99% 12.431% 9 37.862 3573 3582 3600 rBV2 435793 1297220 38.01% 6.949%

Sum of corrected areas: 18668555

9447.D GCMS0507.M Thu May 09 14:42:50 2002

NYC-WTC_000045467

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NYC-WTC_000045467Source: NYC Law Department, mirrored locally

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