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GCMS re-analysis comments for sample AE09391, May 2002

Machine-extracted title · confidence 100%

Laboratory notes describing re-extraction and re-analysis of sample AE09391 due to initial recovery issues on May 15, 2002.

NYC-WTC_000045443–000045451

Folder label: “GCMS X 5/3/02 A 5/8/02

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Scanned page image, NYC-WTC_000045448
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\1\DATA\MAY0802\9391.D Vial: 8 Acq On 8 May 2002 5:24 pm Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 ■ Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.153 337 340 372 rVB 482207 1094901 29.06% 5.967% 2 12.194 775 781 796 rBV 1178773 2646466 70.24% 14.423% 3 15.823 1171 1177 1188 rBV 1646180 3359537 89.16% 18.310% 4 21.128 1749 1756 1776 rBV 1749953 3767891 100.00% 20.535% 5 23.273 1981 1990 1998 rBV2 183694 406312 10.78% 2.214%

6 25.573 2235 2241 2251 rW2 1584011 3386024 89.87% 18.454% 7 33.627 3113 3120 3140 rBV2 915899 2149165 57.04% 11.713% 8 37.861 3574 3582 3600 rBV2 514195 1538056 40.82% 8.383%

Sum of corrected areas: 18348352

9391.D GCMS0507.M Thu May 09 14:42:37 2002

NYC-WTC_000045448

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NYC-WTC_000045448Source: NYC Law Department, mirrored locally

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