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GCMS calibration data for TCLP method, May 2002

Machine-extracted title · confidence 100%

GCMS calibration table and instrument data for TCLP analysis recorded on May 5-7, 2002.

NYC-WTC_000022909–000022915

Folder label: “GCMS X 5/8/02 A 5/10/02

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Scanned page image, NYC-WTC_000022912
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\MAY0302\9332.D Vial: 34 Acq On 5 May 2002 12:22 am Operator: Sample RE-EXT. Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.158 336 340 366 rBV 410145 977654 26.94% 5.177% 2 12.190 774 780 796 rBV 1134173 2605307 71.79% 13.795% 3 15.828 1171 1177 1194 rBV 1630919 3309007 91.18% 17.521% 4 21.134 1749 1756 1770 rBV 1758942 3629173 100.00% 19.217% 5 23.269 1983 1989 1996 rVB 95398 186111 5.13% 0.985%

6 25.578 2234 2241 2251 rBV2 1616538 3392688 93.48% 17.964% 7 33.633 3113 3120 3139 rBV2 1088388 2498377 68.84% 13.229% 8 33.853 3139 3144 3159 rVB 150161 367484 10.13% 1.946% 9 37.866 3573 3582 3599 rBV2 650042 1919900 52.90% 10.166%

Sum of corrected areas: 18885701

9332.D GCMS0501.M Tue May 07 12:01:45 2002

NYC-WTC_000022912

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NYC-WTC_000022912Source: NYC Law Department, mirrored locally

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