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GCMS sample analysis summary, May 7, 2002

Machine-extracted title · confidence 90%

Summary of GC/MS analytical results for sample AE08838 processed on May 7, 2002, including surrogate recovery data.

NYC-WTC_000043667–000043677

Folder label: “GCMS X 4/24/02 A 5/3/02

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Scanned page image, NYC-WTC_000043672
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document LSC Area Percent Report

Data File C:\HPCHEM\l\DATA\MAY0302\8838.D Vial: 7 Acq On 3 May 2002 7:55 pm Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 6.354 139 143 150 rBV 21206 39190 1.10% 0.220% 2 8.159 336 340 346 rBV 448080 881270 24.80% 4.945% 3 12.191 774 780 795 rBV 1110044 2573511 72.41% 14.442% 4 14.793 1059 1064 1070 rBV 135861 260765 7.34% 1.463% 5 15.829 1170 1177 1193 rBV 1586406 3249579 91.43% 18.236%

6 21.135 1749 1756 1765 rBV 1773958 3554051 100.00% 19.944% 7 23.270 1982 1989 1995 rVB 161153 318111 8.95% 1.785% 8 25.579 2234 2241 2252 rBV2 1566890 3263917 91.84% 18.316% 9 33.634 3114 3120 3136 rBV2 956033 2154400 60.62% 12.090% 10 37.867 3574 3582 3599 rBV2 524408 1525100 42.91% 8.558%

Sum of corrected areas: 17819894

8838.D GCMS0501.M Mon May 06 10:48:35 2002

NYC-WTC_000043672

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NYC-WTC_000043672Source: NYC Law Department, mirrored locally

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