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← Document results/DEP Box 18/GCMS X 5/8/02 A 5/10/02
Document / 7 pages

GCMS calibration table review, April 2002

Machine-extracted title · confidence 100%

Reviewed data file listing retention times and response factors for deuterated internal standards.

NYC-WTC_000022812–000022818

Folder label: “GCMS X 5/8/02 A 5/10/02

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Scanned page image, NYC-WTC_000022815
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C : \HPCHEM\ 1\DATA\MAYO3029151.D Vial: 30 Acq On 4 May 2002 8:27 pm Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 8.162 337 341 372 rVB 458948 1030429 27.32% 5.363% 2 12.194 775 781 795 rBV 1163697 2673748 70.89% 13.917% 3 15.823 1171 1177 1190 rBV 1630019 3380722 89.63% 17.596% 4 21.138 1750 1757 1772 rBV 1769917 3771803 100.00% 19.632% 5 23.273 1982 1990 1996 rBV 117666 238063 6.31% 1.239% 6 25.573 2234 2241 2252 rBV2 1611241 3476225 92.16% 18.093% 7 33.637 3114 3121 3137 rBV2 1119610 2508962 66.52% 13.059% 8 33.857 3140 3145 3160 rVB 94749 227665 6.04% 1.185% 9 37.862 3574 3582 3596 rBV2 646227 1905079 50.51% 9.916%

Sum of corrected areas: 19212696 9151.D GCMS0501.M Tue May 07 12:01:08 2002

NYC-WTC_000022815

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NYC-WTC_000022815Source: NYC Law Department, mirrored locally

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