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GCMS blank analysis results, sample AE09331, May 2002

Machine-extracted title · confidence 100%

Laboratory report showing non-detect levels for various volatile organic compounds in a method blank.

NYC-WTC_000022719–000022733

Folder label: “GCMS X 5/8/02 A 5/10/02

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Scanned page image, NYC-WTC_000022732
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\050902\508LB.D Vial: 15 Acq On : 10 May 2002 3:31 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 5 2,2’-Binaphthalene, 1,1',2,. Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

34.96 0.32 ug/L 209844 Perylene-dl2 34.70

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,2'-Binaphthalene, 1,1',2,2',3,...262 C20H22 027426-98-8 9 2 2-Bromo-4,6-difluoroaniline 207 C6H4BrF2N 000444-14-4) 3 2-Oxo-4,5-diphenyladipic acid, m... 326 C19H1805 1000200-98-5 9 4 2H-1,3-Thiazine-6-carboxylic aci... 262 C12H1ON203S 016238-38-3 7 Abundance Scan 5426 (34.960 min): 508LB.D (-5422) (-) m/z 131.50 100.00% 131

209 262 5000 40 191 116 34.60 34.80 35.00 35.20 | 281 m/z 209.20 0- 11111111111117 I’ TTTTTTUTTTTTTTTTITOTOugum 56.69% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #59484:2,2'-Binaphthalene, 1,1*,2,2’,3,3’,4,4’-octahydro- 131

5000 262 104 34.60 34.80 35.00 35.20 m/z 118.10 52.49% 15 39 63 78 0- 1c rh lstha । th 111' 4.4.157.178.202 219234 . " " i" " i" " i1' miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #85327: 2-Bromo-4,6-difluoroaniline 209

34.60 34.80 35.00 35.20 5000 108 128 m/z 262.10 51.18%

31 za 64 81 179 n 0- —444—ll TT‘ TTTTTgtTTTT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #59451:2-Oxo-4,5-diphenyladipic acid, methyl ester 131 34.60 34.80 35.00 35.20 m/z 191.00 45.14% 191 5000 91 59 11 .165 ।

miz-> 0 39 i ,, j ip r* 141 20 40 +44 7 A, r ITH4149+4+ 1,206221 249,267 298 326 Ti" ... [ dual Pi I < 11 < j < > । >'[ 111111-.. 60 80 100 120 140 160 180 200 220 240 260 280 300 320 4 I ' 1 ‘ 1 I ' 34.60 34.80 35.00 35.20

508LB.D 050102.M Mon May 13 11:26:47 2002 Page 7

NYC-WTC_000022732

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NYC-WTC_000022732Source: NYC Law Department, mirrored locally

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