Volatile organic compounds results, Mar 13 2002

NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\02MAR13\0313C10C.D Vial: 3 Acq On : 14 Mar 2002 5:10 am Operator: 201-wb Sample : cal 10 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Mar 14 11:17 2002 Quant Results File: HP022702.RES Quant Method : C:\HPCHEM\1\METHODS\HP022702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Wed Mar 13 14:51:22 2002 Response via : Initial Calibration DataAcq Meth : HP022702

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.14 114 1763374 5.00 ug/L -0.04 24) CHLOROBENZENE-D5 21.79 117 1631640 5.00 ug/L -0.04 52) 1,4-DICHLOROBENZENE-D4 26.97 152 825704 5.00 ug/L -0.04 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.37 65 722184 6.33 ug/L -0.04 Spiked Amount 5.000 Recovery = 126.60% 3) 4-BROMOFLUOROBENZENE 24.38 174 676424 4.74 ug/L -0.04 Spiked Amount 5.000 Recovery = 94.80% 25) TOLUENE-D8 18.49 98 2084458 5.30 ug/L -0.04 Spiked Amount 5.000 Recovery = 106.00% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.90 85 436562 9.00 ug/L 99 5) CHLOROMETHANE 5.54 50 549057 10.40 ug/L 97 6) VINYL CHLORIDE 5.64 62 373945 11.08 ug/L 95 7) BROMOMETHANE 6.63 94 396901 11.83 ug/L 94 8) CHLOROETHANE 6.76 64 375142 12.76 ug/L 95 9) TRICHLOROFLUOROMETHANE 7.32 101 776126 12.00 ug/L 98 12) ACETONE 8.31 43 107033 11.86 ug/L 96 13) 1,1-DICHLOROETHENE 8.65 61 1091347 14.21 ug/L 97 14) METHYLENE CHLORIDE 9.65 49 949239 10.49 ug/L 96 15) METHYL TERT BUTYL ETHER 9.96 73 1030407 9.93 ug/L 95 16) TRANS-1,2-DICHLOROETHENE 10.32 61 1109361 10.66 ug/L 100 17) 1,1-DICHLOROETHANE 11.20 63 1291538 10.04 ug/L 98 18) 2-BUTANONE (MEK) 12.04 43 131166 6.79 ug/L 91 19) 2,2-DICHLOROPROPANE 12.43 77 778554 8.21 ug/L 96 20) CIS-1,2-DICHLOROETHENE 12.51 96 787656 9.95 ug/L 98 21) CHLOROFORM 12.85 83 1408160 10.43 ug/L 99 22) BROMOCHLOROMETHANE 13.23 49 548443 8.24 ug/L 95 23) 1,2-DICHLOROETHANE 14.57 62 947060 11.10 ug/L 97 26) 1,1,1-TRICHLOROETHANE 13.74 97 1109332 12.71 ug/L 99 27) 1,1-DICHLOROPROPENE 14.06 75 993017 11.61 ug/L 98 28) CARBON TETRACHLORIDE 14.34 117 961970 13.14 ug/L 99 29) BENZENE 14.68 78 2499704 10.33 ug/L 99 30) TRICHLOROETHENE 15.94 95 783546 11.01 ug/L 98 31) 1,2-DICHLOROPROPANE 16.29 63 627241 8.93 ug/L 100 32) DIBROMOMETHANE 16.97 174 367250 9.97 ug/L 97 33) BROMODICHLOROMETHANE 16.82 83 965821 10.96 ug/L 97 34) 2-CHLOROETHYL VINYL ETHER 17.30 63 206493 9.27 ug/L 96 35) METHYL ISO-BUTYL KETONE 17.38 58 102844 8.22 ug/L 88 36) CIS-1,3-DICHLOROPROPENE 17.91 75 889859 9.29 ug/L 98 37) TOLUENE 18.66 91 2694008 10.13 ug/L 99 3 8) TRANS-1,3-DICHLOROPROPENE 18.93 75 651130 9.50 ug/L 98 39) 1,1,2-TRICHLOROETHANE 19.32 97 420466 9.20 ug/L 98 40) TETRACHLOROETHENE 20.11 166 789529 10.34 ug/L 99 41) 1,3-DICHLOROPROPANE 19.85 76 778866 9.30 ug/L 100 42) DIBROMOCHLOROMETHANE 20.55 129 562484 10.26 ug/L 99 43) 1,2-DIBROMOETHANE 20.99 107 436303 9.38 ug/L 99 44) CHLOROBENZENE 21.88 112 1784604 9.79 ug/L 97 45) 1,1,1,2-TETRACHLOROETHANE 21.93 131 634138 10.49 ug/L 98 46) 2-HEXANONE 19.22 43 172241 5.41 ug/L 93 47) ETHYLBENZENE 21.91 91 3187775 10.56 ug/L 98 48) P & M-XYLENE 22.07 106 2141844 19.69 ug/L 91 (#) = qualifier out of range (m) = manual integration 0313C10C.D HP022702.M Thu Mar 14 11:17:27 2002 Page 1

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