VOC analysis results, sample AE03507, Feb 22 2002

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\02feb22\0221R5A.D Vial: 5 Acq On : 22 Feb 2002, 12:43 pm Operator: 201-wb Sample : ref 5 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 22 13:21 2002 Quant Results File: HP021702.RES Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Tue Feb 19 16:16:43 2002 Response via : Initial Calibration DataAcq Meth : HP021702

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.12 114 2563978 5.00 ug/L 0.00 24) CHLOROBENZENE-D5 21.78 117 2478457 5.00 ug/L 0.02 52) 1,4-DICHLOROBENZENE-D4 26.97 152 1274351 5.00 ug/L 0.02 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.35 65 815928 4.18 ug/L 0.00 Spiked Amount 5.000 Recovery = 83.60% 3) 4-BROMOFLUOROBENZENE 24.36 174 949341 4.93 ug/L 0.00 Spiked Amount 5.000 Recovery = 98.60% 25) TOLUENE-D8 18.49 98 3145775 5.12 ug/L 0.02 Spiked Amount 5.000 Recovery = 102.40% Target Coinpounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.88 85 302522 3.35 ug/L 99 5) CHLOROMETHANE 5.52 50 254336 2-99 ug/D ug/L 97 6) VINYL CHLORIDE 5.64 62 204745 (6.44 99 < -s6 7) BROMOMETHANE 6.62 94 205221 4791 ug/L 97 8) CHLOROETHANE 6.76 64 214873 5.09 ug/L 92 9) TRICHLOROFLUOROMETHANE 7.31 101 445187 5.50 ug/L 97 12) ACETONE 8.29 43 76029 4.31 ug/L 97 13) 1,1-DICHLOROETHENE 8.63 61 547554 4.44 ug/L 98 14) METHYLENE CHLORIDE 9.64 49 816011 5.51 ug/L 99 15) METHYL TERT BUTYL ETHER 9.94 73 751618 4.59 ug/L 96 16) TRANS-1,2-DICHLOROETHENE 10.30 61 861268 5.46 ug/L 99 17) 1,1-DICHLOROETHANE 11.19 63 1032078 554 uq/L 96 18) 2-BUTANONE (MEK) 12.02 43 141823 Q. 47 ug/D 19) 2,2-DICHLOROPROPANE 12.41 77 771429 5.16 ug/L 96 20) CIS-1,2-DICHLOROETHENE 12.50 96 630556 5.93 ug/L 96 21) CHLOROFORM 12.84 83 1056107 5.64 ug/L 94 22) BROMOCHLOROMETHANE 13.21 49 506120 5.69 ug/L 99 23) 1,2-DICHLOROETHANE 14.56 62 627013 4.98 ug/L 99 26) 1,1,1-TRICHLOROETHANE 13.74 97 779600 5.64 ug/L 96 27) 1,1-DICHLOROPROPENE 14.06 75 819150 5.94 ug/L 96 28) CARBON TETRACHLORIDE 14.32 117 662152 5.89 ug/L 99 29) BENZENE 14.66 78 2211807 6.18 ug/L 99 30) TRICHLOROETHENE 15.94 95 663720 6.20 ug/L 89 31) 1,2-DICHLOROPROPANE 16.29 63 607326 6.00 ug/L 97 32) DIBROMOMETHANE 16.96 174 300304 6.25 ug/L 94 33) BROMODICHLOROMETHANE 16.81 83 732557 5.66 ug/L 98 34) 2-CHLOROETHYL VINYL ETHER 17.28 63 192440 5.14 ug/L 98 35) METHYL ISO-BUTYL KETONE 17.37 58 98343 5.31 ug/L 99 36) CIS-1,3-DICHLOROPROPENE 17.89 75 819395 5.74 ug/L 99 37) TOLUENE 18.66 91 2434499 6.51 ug/L 99 38) TRANS-1,3-DICHLOROPROPENE 18.93 75 570818 5.46 ug/L 97 39) 1,1,2-TRICHLOROETHANE 19.32 97 373131 6.15 ug/L 98 40) TETRACHLOROETHENE 20.11 166 715740 7.03 ug/L 98 41) 1,3-DICHLOROPROPANE 19.85 76 691959 5.83 ug/L 98 42) DIBROMOCHLOROMETHANE 20.55 129 434913 5.96 ug/L 99 43) 1,2-DIBROMOETHANE 20.99 107 374449 5.70 ug/L 94 44) CHLOROBENZENE 21.88 112 1645827 6.89 ug/L 94 45) 1,1,1,2-TETRACHLOROETHANE 21.91 131 528066 6.60 ug/L 98 46) 2-HEXANONE 19.22 43 195284 5.25 ug/L 97 47) ETHYLBENZENE 21.91 91 2877490 6.67 ug/L 96 48) P & M-XYLENE 22.07 106 2053419 13.95 ug/L 90 (#) = qualifier out of range (m) = manual integration 0221R5A.D HP021702.M Fri Feb 22 13:21:46 2002 Page 1

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