VOC analysis results, sample AE03958, Feb 19 2002

NYC 9/11 Public Portal Document Quantitation Report (Not Reviewed) Data File : C:\HPCHEM\1\DATA\02FEB19\0219R5A.D Vial: 1 Acq On : 19 Feb 2002 5:55 pm Operator: 201-wb Sample : ref 5 Inst : GC/MS Ins Mise : February 19, 2002 Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Feb 20 8:33 2002 Quant Results File: HP021702.RES Quant Method : C:\HPCHEM\1\METHODS\HP021702.M (RTE Integrator) Title : VOCs BY EPA METHOD 524 Last Update : Wed Feb 20 08:33:37 2002 Response via : Initial Calibration DataAcq Meth : HP021702

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-DIFLUOROBENZENE 15.09 114 1753097 5.00 ug/L -0.03 24) CHLOROBENZENE-D5 21.73 117 1662755 5.00 ug/L -0.04 52) 1,4-DICHLOROBENZENE-D4 26.92 152 796147 5.00 ug/L -0.03 System Monitoring Compounds 2) 1,2-DICHLOROETHANE-D4 14.32 65 591200 4.43 ug/L -0.03 Spiked Amount 5.000 Recovery = 88.60% 3) 4-BROMOFLUOROBENZENE 24.31 174 582969 4.42 ug/L -0.04 Spiked Amount 5.000 Recovery = 88.40% 25) TOLUENE-D8 18.44 98 2168504 5.26 ug/L -0.03 Spiked Amount 5.000 Recovery = 105.20% Target Compounds Qvalue 4) DICHLORODIFLUOROMETHANE 4.86 85 219481 3.55 ug/L 99 5) CHLOROMETHANE 5.50 50 237871 4.61 ug/L 99 6) VINYL CHLORIDE 5.60 62 162146 5.13 ug/L 97 7) BROMOMETHANE 6.57 94 140467 4.92 ug/L 98 8) CHLOROETHANE 6.71 64 132516 4.59 ug/L 96 9) TRICHLOROFLUOROMETHANE 7.28 101 259465 4.68 ug/L 100 12) ACETONE 8.24 43 40209 3.66 ug/L 94 13) 1,1-DICHLOROETHENE 8.60 61 315533 3.74 ug/L 96 14) METHYLENE CHLORIDE 9.60 49 542131 5.35 ug/L 98 15) METHYL TERT BUTYL ETHER 9.91 73 371217 3.54 ug/L 94 16) TRANS-1,2-DICHLOROETHENE 10.27 61 424832 3.94 ug/L 100 17) 1,1-DICHLOROETHANE 11.15 63 547356 4.30 ug/L 99 18) 2-BUTANONE (MEK) 11.99 43 92157 3.63 ug/L 97 19) 2,2-DICHLOROPROPANE 12.36 77 400099 3.91 ug/L 97 20) CIS-1,2-DICHLOROETHENE 12.46 96 338296 4.65 ug/L 99 21) CHLOROFORM 12.80 83 580815 4.54 ug/L 97 22) BROMOCHLOROMETHANE 13.18 49 281747 4.63 ug/L 96 23) 1,2-DICHLOROETHANE 14.52 62 368661 4.28 ug/L 100 26) 1,1,1-TRICHLOROETHANE 13.69 97 402253 4.34 ug/L 98 27) 1,1-DICHLOROPROPENE 14.01 75 429044 4.64 ug/L 97 28) CARBON TETRACHLORIDE 14.27 117 324516 4.31 ug/L 98 29) BENZENE 14.61 78 1191137 4.96 ug/L 99 30) TRICHLOROETHENE 15.89 95 358281 4.99 ug/L 94 31) 1,2-DICHLOROPROPANE 16.24 63 355345 5.23 ug/L 96 32) DIBROMOMETHANE 16.91 174 147506 4.58 ug/L 91 33) BROMODICHLOROMETHANE 16.75 83 413641 4.76 ug/L 100 34) 2-CHLOROETHYL VINYL ETHER 17.25 63 93684 3.73 ug/L 100 35) METHYL ISO-BUTYL KETONE 17.32 58 50930 4.10 ug/L 97 36) CIS-1,3-DICHLOROPROPENE 17.84 75 468942 4.90 ug/L 98 37) TOLUENE 18.61 91 1337540 5.33 ug/L 99 38) TRANS-1,3-DICHLOROPROPENE 18.88 75 344815 4.91 ug/L 99 39) 1,1,2-TRICHLOROETHANE 19.27 97 212201 5.22 ug/L 99 40) TETRACHLOROETHENE 20.06 166 352617 5.16 ug/L 98 41) 1,3-DICHLOROPROPANE 19.80 76 395442 4.96 ug/L 99 42) DIBROMOCHLOROMETHANE 20.48 129 235583 4.81 ug/L 100 43) 1,2-DIBROMOETHANE 20.94 107 208156 4.72 ug/L 98 44) CHLOROBENZENE 21.81 112 888121 5.54 ug/L 96 45) 1,1,1,2-TETRACHLOROETHANE 21.86 131 281142 5.24 ug/L 96 46) 2-HEXANONE 19.17 43 91031 3.65 ug/L 97 47) ETHYLBENZENE 21.86 91 1610821 5.57 ug/L 98 48) P & M-XYLENE 22.02 106 1117560 11.32 ug/L 93 (#) = qualifier out of range (m) = manual integration 0219R5A.D HP021702.M Wed Feb 20 10:12:14 2002 Page 1

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