GCMS analysis results, sample AD30936, January 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\JAN2502\30936A.D Vial: 3 Acq On : 25 Jan 2002 11:09 am Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 11.25 0.30 ug/1 89474 1,4-Dichlorobenzene-d4 11.48 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 72 2“ l-Propanol, 2-(2-hydroxypropoxy) - 134C6H14O3 000106-62-7 42 3 2-Propanol, 1,1' - 1-methyl-1,2-eth 192 C9H20O4 001638-16-0 40 4 2-Propanol, 1,11- oxybis- 134 C6H14O3 000110-98-5 36 Abundance an 676 (11.249 min): 30936A.D (-) m/z 59.05 100.00% 59

m/z-> 5000

Abundance -r-p-n-r-p- 20 30 +31,4-51-4 40 50 60 45

70 80 90 100 110 120 130 73

#9238:2-Propanol, 1-(2-methoxy-1-methylethoxy)- 103

i ■ ■111 ■ ■ ■ • । •1 m/z MN 11.00 11.20 11.40 11.60 44.9 58.42%

5000 103 14 * ** i i i 45 11.00 11.20 11.40 11.60 73 31 m/z 103.05 32.17% PPP ! * > * * i * +1 130 • i • • • ■ 18* ■ • । ■ *1’’I+’1** miz-> 20 30 40 50 (60 70 80 90 100 110 120 130 Abundance #6086; 1-Propanol, 2-{2-hydroxypropoxy)- 59 A 11.00 11.20 11.40 11.60 5000 m/z 73.00 29.63%

M 31 45 103

T 75 89 p-rT-rr-p-rT-p-rT-rT-p-r-r-p-rT-T-p-T-rT-p-rT-TT-p-rT-p-r-r miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #20630: 2-Propanol, 1,1'-[(1-methyl-1,2-ethanediyl)bis(oxy) 59 11.00 11.20 11.40 11.60 m/z 41.05 29.53% 5000 31 45 103 39 1- ■ I u ill) ■ ■ ■ ' i 73 • । ■ ■ ' ■ i ■ ■ ■ ''i ■ I, ' ' • ' i ■ ■ ■ ■ i ' ' ■ ■ i ‘ 1 ■ » । 117 । । ' i j • ■ AAA/,

m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 11.00 11.20 11.40 11.60

30936A.D GCMS1126.M Fri Jan 25 12:23:50 2002 Page 3

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