DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2 502\30649.D Vial: 34 Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-l-met Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

11.24 0.25 ug/1 183305 1,4-Dichlorobenzene-d4 11.48

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanol, 1-(2-methoxy- 1-methylet 148 C7H16O3 020324-32-7 72 2 1-Propanol, 2-(2-hydroxypropoxy)- 134 C6H14O3 000106-62-7 53 3 2-Butanol, 3,3'-oxybis- 162 C8H18O3 054305-61-2 50 4 Ethane/ 1-ethoxy-l-methoxy­ 104 C5H12O2 _______ 010471-14-4 43 Abundance / Scan 675 (11.244 min): 30649.D(-) m/z 59.05 100.00% ( 59 5000 45 M) N 73 103

....... > , 51 . , 67 , 11.00 11.20 11.40 11.60 85 i 1,11 ■1111' ■ ■ ■ r'1 ■ i 1 ' ‘ 1 i ' m/z 44.95 49.69% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1 -methylethoxy) 59

5000 103 45 73 11.00 11.20 11.40 11.60 31 m/z 103.00 31.81% 1,,.. 1,., , , , I J, 'i1111111 .......... !......... 130.... m/z-> 20 30 40 50 (60 70 80 90 100 110 120 130 140 Abundance #6086: 1-Fropanol 2-(2-nydroxypropoxy)- 59 ' '>1 ' ' 11.00 11.20 11.40 11.60 5000 73.00 m/z __ 27.33% 31 45 103

75 89 m/z-> 20__ 30 40 50 60 70__ 80__ 90 100 110 120 130 140 Abundance #12859: 2-Butanol, 3,3’-oxybis- 59 11.00 11.20 11.40 11.60 m/z 41.05 26.72%

m/z-> 5000

.

20 31

30 40 45

1 ■

50 i ■ I ■

60 ■ ■ ■ i

70 ■ ■ ■ ■

80 i ■ ■ ■ ■ i

90 ■ ■ ■ 103

■ i ■

100 ’10D0—TmB//nL.n 110 120 134 130 140 NWV 11.00 11.20 11.40 11.60

30649.D GCMS1126.M Mon Jan 28 12:18:00 2002 Page 2

NYC-WTC_000004255