NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\JAN2 502\30649.D Vial: 34
Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS
Sample : REINJECT Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
14.13 1.64 ug/1 1417210 Naphthalene-d8 15.09
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasilo: he, decamethyl- 370 C10H3005Si5 000541-02-6 50
2 Benzoic acid,/ ,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 47
3 3,4-Dihydro: ybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43
4 Benzoic aci , 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40
Abundance Scan 989 (14.127 min): 30649.D (-) m/z 73.00 100.00%
73
5000
267
355
45 133 154[ . 177 251 13.80 14.00 14.20 14.40
89 108J 193208223
i
m/z->
I
■ ■ ।■ i ■ ■" । । 44+293323339
. ilt i T | | i". i i । i i i .'।
40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
m/ z 266.9 31.88%
Abundance #51266: Cyclopentasiloxane, decamethyl-
73
355
267
5000
13.80 14.00 14.20 14.40
m/z 355.05 21.88%
191207 251 1 323339
I " “ I' *'11 TWIm9muumu*nnmaTT 1 ’ " 11
m/z-> 11 ‘'11'1 ■ ■ I'1'11 ‘11 ‘ I
40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #75978: Benzoic acid. 2,5-bist trimethylsilox)- trimethyls
t 73
355
13.80 14.00 14.20 14.40
5000 m/z 268.00 8.40%
45
I i , 147 179 207223 267282297 I 370
" i ■ ■ ■ ■ i ■ ■ ■ ■ i'1 4
'' i'''11" '' i'''' i'' " i ■ ■' ■ i'''' i' ■'' i' " ' I ‘1 ‘' I " “ i1'1' i''' ■ i ‘
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360
Abundance #49868: 3,4-Dihydroxybenzyi alcohol, tris(trimethylsilyl)-
73 13.80 14.00 14.20 14.40
m/z 74.00 8.24%
267
5000 179
356
45 147
" i ■'' ''l'
209 237 312 341
i " '' i ‘ ■ i ■'1 ■ i'T' ■ i ■ " 11 ■ " ■ i " ■' i1'
" i'''' i ■' " i ■' " I " ■' i'11' I ‘ i' ■ ■ ■ i
m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 13.80 14.00 14.20 14.40
30649.D GCMS1126.M Mon Jan 28 12:18:04 2002 Page 3
NYC-WTC_000004256
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