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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004256
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2 502\30649.D Vial: 34 Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

14.13 1.64 ug/1 1417210 Naphthalene-d8 15.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasilo: he, decamethyl- 370 C10H3005Si5 000541-02-6 50 2 Benzoic acid,/ ,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 47 3 3,4-Dihydro: ybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 4 Benzoic aci , 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 40 Abundance Scan 989 (14.127 min): 30649.D (-) m/z 73.00 100.00% 73

5000 267 355 45 133 154[ . 177 251 13.80 14.00 14.20 14.40 89 108J 193208223 i m/z-> I ■ ■ ।■ i ■ ■" । । 44+293323339 . ilt i T | | i". i i । i i i .'। 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 m/ z 266.9 31.88% Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 13.80 14.00 14.20 14.40 m/z 355.05 21.88% 191207 251 1 323339 I " “ I' *'11 TWIm9muumu*nnmaTT 1 ’ " 11 m/z-> 11 ‘'11'1 ■ ■ I'1'11 ‘11 ‘ I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #75978: Benzoic acid. 2,5-bist trimethylsilox)- trimethyls t 73 355 13.80 14.00 14.20 14.40 5000 m/z 268.00 8.40% 45 I i , 147 179 207223 267282297 I 370 " i ■ ■ ■ ■ i ■ ■ ■ ■ i'1 4 '' i'''11" '' i'''' i'' " i ■ ■' ■ i'''' i' ■'' i' " ' I ‘1 ‘' I " “ i1'1' i''' ■ i ‘ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyi alcohol, tris(trimethylsilyl)- 73 13.80 14.00 14.20 14.40 m/z 74.00 8.24% 267 5000 179 356 45 147 " i ■'' ''l' 209 237 312 341 i " '' i ‘ ■ i ■'1 ■ i'T' ■ i ■ " 11 ■ " ■ i " ■' i1' " i'''' i ■' " i ■' " I " ■' i'11' I ‘ i' ■ ■ ■ i m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 13.80 14.00 14.20 14.40

30649.D GCMS1126.M Mon Jan 28 12:18:04 2002 Page 3

NYC-WTC_000004256

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NYC-WTC_000004256Source: NYC Law Department, mirrored locally

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