NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\JAN2502\30649.D Vial: 34
Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS
Sample : REINJECT Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3 - Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.27 6.20 ug/1 5353830 Naphthalene-d8 15.09
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,77Heptamethy1-3,3-bis(t 444 C13H4005Si6 038147-00-1 35
2 2H-1,4-Benzodlazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22
3 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12
4 Pregnane-3,/0-dione, 11-[(trimethyl 462 C26H46N2O3Si 057305-27-8 7
Abundance Scan 1331 (17.266 min): 30649.D (-) m/ z 73.0,0 100 .00%
73
5000
341
147 429
45 17.00 17.20 17.40 17.60
, 96 117 [ 179 207225 251 281 311 [ t 367
0-TOUCCmmumuTu 397 L
I . . . I | H . , 1 . . , , | , Il . ( . . m/z 341.00 32.60%
miz-> 40 60 80 100120140160180200220240260280300320340360380400420440
Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxyjt
73
147
5000 267
355 429 17.00 17.20 17.40 17.60
45 207 m/z 147.00 14.81%
m/z->
....।....।....।.... ।.... ।,. Htt
40 60 80 100120140160180200220240260280300320340360380400420440
‘ ‘-1‘‘11/1141*11/171117
Abundance #48337: 244-1 4-Benzediazepin 2 one 7-chiom 1.3-dihydro-5
73 341
17.00 17.20 17.40 17.60
5000 m/z 342.00 10.96%
45
91
116 146 227 269 315
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 ................. .............................
Abundance #73587: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl-
73 239 17.00 17.20 17.40 17.60
m/z 325.00 10.84%
342
5000
45
133
I , 211
m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 17.00 17.20 17.40 17.60
30649.D GCMS1126.M Mon Jan 28 12:18:09 2002 Page 4
NYC-WTC_000004257
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