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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004257
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2502\30649.D Vial: 34 Acq On : 25 Jan 2002 9:55 pm Operator: 209 GALOS Sample : REINJECT Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3 - Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

17.27 6.20 ug/1 5353830 Naphthalene-d8 15.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,1,1,5,7,7,77Heptamethy1-3,3-bis(t 444 C13H4005Si6 038147-00-1 35 2 2H-1,4-Benzodlazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 3 Silane, [1,2,3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 12 4 Pregnane-3,/0-dione, 11-[(trimethyl 462 C26H46N2O3Si 057305-27-8 7 Abundance Scan 1331 (17.266 min): 30649.D (-) m/ z 73.0,0 100 .00% 73

5000 341 147 429 45 17.00 17.20 17.40 17.60 , 96 117 [ 179 207225 251 281 311 [ t 367 0-TOUCCmmumuTu 397 L I . . . I | H . , 1 . . , , | , Il . ( . . m/z 341.00 32.60% miz-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxyjt 73

147 5000 267 355 429 17.00 17.20 17.40 17.60 45 207 m/z 147.00 14.81%

m/z-> ....।....।....।.... ।.... ।,. Htt 40 60 80 100120140160180200220240260280300320340360380400420440 ‘ ‘-1‘‘11/1141*11/171117

Abundance #48337: 244-1 4-Benzediazepin 2 one 7-chiom 1.3-dihydro-5 73 341

17.00 17.20 17.40 17.60 5000 m/z 342.00 10.96% 45 91 116 146 227 269 315 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 ................. ............................. Abundance #73587: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- 73 239 17.00 17.20 17.40 17.60 m/z 325.00 10.84% 342 5000

45 133 I , 211 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 17.00 17.20 17.40 17.60

30649.D GCMS1126.M Mon Jan 28 12:18:09 2002 Page 4

NYC-WTC_000004257

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NYC-WTC_000004257Source: NYC Law Department, mirrored locally

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