NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30907.D Vial: 43
Acq On 2 Jan 2002 5:37 am Operator: 209 GALOS
Sanpl e gems scan 12/19a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 9 3-1sopropoxy-1,1,1,7,7,7-hexam Concentrat ion Rank 7
R.T. EstConc Area Relative to ISTD R.T.
26.90 0.71 ug/1 197305 Phenanthrene-dl0 24.99
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Isopropoxy-1,1,1,7,7/7-hexamethyl 576 C18H5207Si7 071579-69-6 50
2 Trisiloxane, 1,1,1,5,5, 5-hexamethyl 384 C12H3604Si5 003555-47-3 40
3 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 33
4 Ethanedioic acid, bis (trimethylsily 234 C8H18O4Si2 018294-04-7 32
Abundance Scan 2380 (26.896 mln): 30907.D (-) m/ z 73.00 100.00%
73
5000
147
221 281 FTLnnn/mdrn1/m/1/n/d/mm.
26.60 26.80 27.00 27.20
TT
45 117. | 1911 I 249, .. 327,355,401 429 ..... m/z 147.00 33.91%
m/z->
Abundance
50 100 150 200 250 300 350 400 450 500
#60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim
550
i 73
5000 26.60 26.80 27.00 27.20
147
221 281
m/z 281.00 18.63%
327 415 519 561
TI - TTnnnnummm"tKtr
miz-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #52459, Trisiloxane, 1,1,1 5,5.5-hexamethyl-3.3-bis[(trimet
73 147
I I l I 3 818s 88E88811I
281 26.60 26.80 27.00 27.20
5000 m/z 221.05 15.78%
207 249 369
— 338 1......................... ..
miz-> 50 100 150 200 250 300 350 400 450 500 550 \
Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether > * i * * > * । * * > * i * » > » i * »
73 26.60 26.80 27.00 27.20
m/z 74.00 8.98%
207
5000 147
34 103 281
395 482
I i I ,
■ • i • ■ ■ • i ■ • •) ■ • ' ■ i ■ • 1 • i 1 1 f ‘ i ■ 1 ■ 1 i ■ * ■ ■ i ■ 1 ; • > ' ' I > । ‘ ' | ' '
miz-> 50 100 150 200 250 300 350 400 450 500 550 26.60 26.80 27.00 27.20
30907.D GCMS1126.M Fri Jan 25 11:36:02 2002 Page 9
NYC-WTC_000018679
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