NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
• Data File C:\HPCHEM\1\DATA\DEC3101\30906.D Vial: 42
Acq On 2 Jan 2002 4:39 am Operator: 209 GALOS
Sample gems scan 12/19a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Jan 25 9:41 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update : Tue Jan 22 11:56:23 2002
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 875524 20.00 ug/1 -0.03
10) Naphthalene-d8 15.28 136 3384384 20.00 ug/1 -0.03
17) Acenaphthene-diO 20.56 164 1716563 20.00 ug/1 -0.02
29) Phenanthrene-dlO 24.98 188 2557715 20.00 ug/1 0.00
38) Chrysene-dl2 33.02 240 1565034 20.00 ug/1 0.00
44) Perylene-dl2 37.12 264 883489 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.06 235 153763 5.47 ug/mL -0.01
Spiked Amount 5.000 Recovery = 109.40%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.24 74 594 N.D.
3) bis(2-Chloroethyl)ether 11.17 93 200 N.D.
4) 1,3-Dichlorobenzene 11.61 146 116 N.D.
5) 1,4-Dichlorobenzene 11.72 146 320 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) 1sophorone 14.10 82 187 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.33 128 2684 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 20.12 163 919 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 20.13 152 954 N.D.
2 3) Acenaphthene 20.66 153 1275 N.D.
24) 2,4-Dinitrotoluene 21.21 165 920 N.D.
25) Diethylphthalate 22.11 149 6107 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 22.25 166 1039 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 22.82 77 264 N.D.
(#) = qualifier out of range (m) = manual integration
30906.D GCMS1126.M Fri Jan 25 09:44:00 2002 Page 1
NYC-WTC_000018652
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