NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\1\DATA\DEC3101\30934.D Vial: 51
Acq On 2 Jan 2002 3:21 pm Operator: 209 GALOS
Sample gems scan 12/19a Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: RTEINT.P
Quant Time: Jan 25 10:10 2002 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update ': Tue Jan 22 11:56:23 2002
Response via : Initial Calibration
DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.68 152 803038 20.00 ug/1 -0.02
10) Naphthalene-d8 15.28 136 3081437 20.00 ug/1 -0.02
17) Acenaphthene-dlO 20.56 164 1552036 20.00 ug/1 -0.01
29) Phenanthrene-diO 24.99 188 2288581 20.00 ug/1 0.00
38) Chrysene-dl2 33.03 240 1335367 20.00 ug/1 0.00
44) Perylene-dl2 37.12 264 749661 20.00 ug/1 0.00
System Monitoring Compounds
37) 2,4-DDD 30.07 235 127017 5.05 ug/mL 0.00
Spiked Amount 5.000 Recovery = 101.00%
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.27 74 501 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 0.00 82 0 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.35 128 566 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chioronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 20.29 163 503 N.D.
21) 2,6-Dinitrotoluene 20.28 165 191 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 21.28 165 293 N.D.
25) Diethylphthalate 22.15 149 1590 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 0.00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
30934.D GCMS1126.M Fri Jan 25 10:13:12 2002 Page 1
NYC-WTC_000018735
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