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GC/MS analysis results for sample AD30934, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.

NYC-WTC_000018733–000018753

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\30934.D Vial: 51 Acq On 2 Jan 2002 3:21 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 25 10:10 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update ': Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.99 178 916 N.D. 34) Anthracene 24.99 178 916 N.D. 35) Di-n-butylphthalate 27.05 149 5948 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.73 149 1092 N.D. 41) Benzo(a)anthracene 33.03 228 4385 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 3748 N.D. 43) Chrysene 33.10 228 1455 N.D. 45) Di-n-Octylphthalate 35.06 149 186 N.D. 4 6) Benzo(b)fluoranthene 36.19 252 2049 N.D. 47) Benzo(k)fluoranthene 36.11 252 581 N.D. 4 8) Benzo(a)pyrene 36.98 252 207 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30934.D GCMS1126.M Fri Jan 25 10:13:16 2002 Page 2

NYC-WTC_000018736

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NYC-WTC_000018736Source: NYC Law Department, mirrored locally

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