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GC/MS analysis results for sample AD30909, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.

NYC-WTC_000018693–000018715

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\30909.D Vial: 52 Acq On 2 Jan 2002 4:19 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 25 10:14 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : : 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.05 178 188 N.D. 34) Anthracene 25.05 178 188 N.D. 35) Di-n-butylphthalate 27.06 149 4516 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 31.72 149 3217 N.D. 41) Benzo(a)anthracene 33.04 228 3342 N.D. 42) Bis(2-ethylhexyl)phthalate 33.31 149 3628 N.D. 43) Chrysene 33.11 228 1529 N.D. 45) Di-n-Octylphthalate 35.08 149 348 N.D. 46) Benzo(b)fluoranthene 36.23 252 1231 N.D. 4 7) Benzo(k)fluoranthene 36.15 252 819 N.D. 48) Benzo(a)pyrene 37.11 252 3177 N.D. 49) Indeno (1, 2,3-cd) pyrene 0.00 276 0 N.D. 50) Dibenz (a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 30909.D GCMS1126.M Fri Jan 25 10:16:17 2002 Page 2

NYC-WTC_000018696

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NYC-WTC_000018696Source: NYC Law Department, mirrored locally

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