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GC/MS analysis results for sample AD30906, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.

NYC-WTC_000018650–000018663

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC3101\30906.D Vial: 42 Acq On 2 Jan 2002 4:39 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 25 9:41 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title .: 209 625/TCLP calibration table Last Update : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.06 178 3505 N.D. 3 4) Anthracene 25.21 178 1240 N.D. 35) Di-n-butylphthalate 27.04 149 23915 N.D. 3 6) Fluoranthene 28.80 202 1135 N.D. 3 9) Pyrene 29.47 202 1960 N.D. 40) Butylbenzylphthalate 31.51 149 3353 N.D. 41) Benzo(a)anthracene 33.11 228 2217 N.D. 42) Bis(2-ethylhexyl)phthalate 33.30 149 26915 0.28 ug/1 95 43) Chrysene 33.11 228 2217 N.D. 45) Di-n-Octylphthalate 35.06 149 751 N.D. 46) Benzo(b)fluoranthene 36.12 252 1036 N.D. 47) Benzo(k)fluoranthene 36.12 252 491 N.D. 4 8) Benzo(a)pyrene 37.14 252 4052 N.D. 4 9) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 5 0) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out.of range (m) = manual integration 30906.D GCMS1126.M Fri Jan 25 09:44:03 2002 Page 2

NYC-WTC_000018653

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NYC-WTC_000018653Source: NYC Law Department, mirrored locally

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