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GC/MS analysis results for sample AD30705, Jan 28 2002

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Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.

NYC-WTC_000018605–000018623

Folder label: “GCMS X 12/19/01 A 1/2/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

. Data- File C:\HPCHEM\1\DATA\DEC3101\30705.D Vial: 46 Acq On 2 Jan 2002 9:30 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Jan 25 9:37 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title .: 209 625/TCLP calibration table Last Update ' : Tue Jan 22 11:56:23 2002 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev (Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 759075 20.00 ug/1 -0.02-- 10) Naphthalene-d8 15.28 136 2898428 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.57 164 1461672 20.00 ug/1 -0.01 29) Phenanthrene-diO 24.99 188 2135100 20.00 ug/1 0.00 38) Chrysene-dl2 33.02 240 1214955 20.00 ug/1 -0.01 44) Perylene-dl2 37.12 264 646885 20.00 ug/1 0.00

System Monitoring Compounds 37) 2,4-DDD 30.07 235 112185 4.78 ug/mL 0.00 Spiked Amount 5.000 Recovery = 95.60%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.31 74 410 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.14 77 222 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 454 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chioronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.28 165 208 N.D. 25) Diethylphthalate 22.14 149 2081 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 22.92 77 171 N.D.

(#) = qualifier out of range (m) = manual integration 30705.D GCMS1126.M Fri Jan 25 09:38:42 2002 Page 1

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