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GCMS analysis results for sample AD30985, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.

NYC-WTC_000018262–000018285

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document LSC Area Percent Report

- Data File C:\HPCHEM\1\DATA\DEC3101\30985.D Vial: 39 Acq On 2 Jan 2002 1:45 am Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.612 276 280 297 rBV 293550 917358 11.26% 1.592% 2 11.128 658 663 673 rBV 350911 864282 10.60% 1.500% 3 11.670 718 722 754 rBV 1926493 5350236 65.64% 9.287% 4 14.305 1000 1009 1019 rBV 1028852 2329338 28.58% 4.043% 5 15.278 1110 1115 1145 rBV 2495820 6724176 82.50% 11.671%

6 17.454 1345 1352 1362 rBV 1546644 3467343 42.54% 6.018% 7 18.161 1423 1429 1435 rBV 94251 214054 2.63% 0.372% 8 20.272 1653 1659 1669 rBV 1058760 2484289 30.48% 4.312% 9 20.557 1684 1690 1716 rBV 2799944 7387615 90.64% 12.823% 10 21.062 1739 1745 1764 rBV2 89667 489196 6.00% 0.849%'

11 22.787 1927 1933 1950 rBV 700230 1586798 19.47% 2.754% 12 24.982 2163 2172 2218 rBV3 2265078 8150298 100.00% 14.147% 13 26.891 2372 2380 2389 rBV 343728 774406 9.50% 1.344% 14 28.654 2564 2572 2579 rBV 277865 612351 7.51% 1.063% 15 30.067 2719 2726 2739 rBV 386274 919766 11.29% 1.596%

16 30.251 2739 2746 2755 rVB 231105 568765 6.98% 0.987% 17 31.720 2899 2906 2920 rVB 206153 553466 6.79% 0.961% 18 33.023 3041 3048 3073 rBV2 1711383 5630064 69.08% 9.772% 19 33.299 3074 3078 3085 rVB 46853 122531 1.50% 0.213% 20 34.373 3189 3195 3209 rBV 114860 373890 4.59% 0.649%

21 35.576 3318 3326 3351 rBV 1564051 4400831 54.00% 7.639% 22 36.714 3444 3450 3464 rBV2 37734 150889 1.85% 0.262% 23 37.118 3486 3494 3523 rBV 933337 3456200 42.41% 5.999% 24 38.008 3585 3591 3601 rBV2 20053 84166 1.03% 0.146%

Sum of corrected areas: 57612308

30985.D GCMS1126.M Wed Jan 23 08:56:44 2002

NYC-WTC_000018267

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NYC-WTC_000018267Source: NYC Law Department, mirrored locally

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