NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 24 pages
GCMS analysis log for sample AD30712, Jan 2002
Machine-extracted title · confidence 100%Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
NYC-WTC_000018214–000018237Folder label: “GCMS X 12/27/01 A 1/16/02”
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NYC 9/11 Public Portal Document Library searen Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30712.D Vial: 35 Acq On 1 Jan 2002 9:53 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 1-Monolinoleoylglycerol trimet Concentration Rank 14
R.T. EstConc Area Relative to ISTD R.T.
36.71 0.59 ug/1 68459 Perylene-d12 37.12
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1 -Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 36 2 Mercaptoacetic acid, bis (trimethyls 236 C8H20O2SSi2 006398-62-5 25 3 3,8-Diowa-2, 9-disiladecane, 2,2,9,9 234 C10H26O2Si2 018001-91-7 25 4 But oic acid, 3-methyl-2-oxo-, bis 260 CllH24O3Si2 072361-19-4 17 Abundance Scan 3449 (36.710 min): 30712.D (-) m/ z 73.00 100.00% 73
147 5000 221 281 51 355 429 36.40 36.60 36.80 37.00 1 ——— ...... . —I ----- m/z 147.0,0 58.20% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58871:1-Monolinoleoylglycerol trimethylsilyl ether 73
207 5000 147 MA,4A,AAA,ATMAAAA 36.40 36.60 36.80 37.00 34 103 m/z 220.95 30.14% 281 I 395 ........ ; - 482 m/z-> 50 100 ‘ ' 150 ' 260 ' 250 300 350 400 450 ' (Abundance #30949: Mercaptoacetic acid, bis(trimethylsifyl)- 73 147 36.40 36.60 36.80 37.00 —A 5000 m/z 281.00 19.00% 221 45 '| 104 193
m/z-> 50 100 150 200 250 300 350 4(X) 450 Abundance #71025:3,8-Dioxa-2,9-disiladecane. 2,2,9,9-tetramethyl- 147 36.40 36.60 36.80 37.00 m/z 355.0 12.45% 5000 116 73 177
miz-> —fuL 50 100 #J 150 ' * i — 200 219 250 300 350 400 450 • • i > • • • i • . • • । 36.40 36.60 36.80 37.00
30712.D GCMS1126.M Wed Jan 23 08:43:42 2002 Page 16
NYC-WTC_000018236
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