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GCMS blank analysis for sample AD30694, Jan 2002

Machine-extracted title · confidence 100%

Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.

NYC-WTC_000018069–000018092

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018073
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NYC 9/11 Public Portal Document

LSC Area Percent Report

' Data File C:\HPCHEM\1\DATA\DEC3101\LBD.D Vial: 26 Acq On 1 Jan 2002 1:10 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 7.617 276 280 293 rBV 361397 1064032 11.97% 1.997% 2 7.764 293 296 311 rVB2 33991 155777 1.75% 0.292% 3 11.133 658 663 671 rBV2 54517 126976 1.43% 0.238% 4 11.674 717 722 749 rBV 2317358 6096913 68.56% 11.440% 5 14.309 1001 1009 1023 rVB 500716 1124718 12.65% 2.110%

6 15.282 1109 1115 1135 rBV 2891537 7527619 84.65% 14.125% 7 17.449 1343 1351 1362 rBV2 1054995 2406903 27.07% 4.516% 8 18.156 1422 1428 1437 rBV 108446 239973 2.70% 0.450% 9 20.276 1653 1659 1670 rBV 842080 1895668 21.32% 3.557% 10 20.561 1683 1690 1706 rBV 3354924 8329726 93.67% 15.630%'

11 20.744 1706 1710 1716 rVB 32662 91943 1.03% 0.173% 12 21.038 1737 1742 1764 rBV 193082 804739 9.05% 1.510% 13 22.792 1927 1933 1947 rVB 555521 1244140 13.99% 2.334% 14 24.986 2163 2172 2206 rBV3 2707010 8892382 100.00% 16.685% 15 26.886 2372 2379 2388 rVB 279931 646300 7.27% 1.213%

16 28.658 2565 2572 2580 rBV 214944 487267 5.48% 0.914% 17 30.062 2720 2725 2736 rBV 412401 950113 10.68% 1.783% 18 30.246 2739 2745 2753 rW 193282 447203 5.03% 0.839% 19 31.715 2899 2905 2914 rBV 158985 397090 4.47% 0.745% 20 33.028 3038 3048 3073 rBV2 1902195 6063763 68.19% 11.378%

21 34.377 3188 3195 3208 rBV 90050 280961 3.16% 0.527% 22 35.571 3317 3325 3336 rBV 56662 194061 2.18% 0.364% 23 36.718 3443 3450 3460 rBV2 28758 109949 1.24% 0.206% 24 37.122 3486 3494 3524 rBV 1018712 3716502 41.79% 6.973%

Sum of corrected areas: 53294718

LBD.D GCMS1126.M Wed Jan 23 09:01:40 2002

NYC-WTC_000018073

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NYC-WTC_000018073Source: NYC Law Department, mirrored locally

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