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GCMS blank analysis for sample AD30694, Jan 2002

Machine-extracted title · confidence 100%

Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.

NYC-WTC_000018069–000018092

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\LBD.D Vial: 26 Acq On 1 Jan 2002 1:10 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 N-(Trifluoracetyl)-0,0',0"-tri Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.79 2.80 ug/1 1244140 Phenanthrene-dl0 24.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-(Trifluoracetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 43 2 Benzoic cid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 38 3 N- (Trif luoroacetyl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 4 Bep eneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 1933 (22.792 mln): LBD.D (-) m/ z 73.00 100.00% 73

5000 .................... .................................. 147 355 221 281 401 22.40 22.60 22.80 23.00 23.20 0- ■ 114 r t 96117. 45 191 , . , 249 , | 327 miz-> 50 100 150 200 250 300 +*r 350 J l 184 400 k . 1 > I 450 i I I I I 500 1 m/z 147.00 26.08% Abundance #58807: N-(Trifluoracetyl)-O,O',O’-tris(trimethylsilyl)epin 73

5000 355 A 22.40 22.60 22.80 23.00 23.20 m/z 355.05 1 ' i 1 1 ' 1 i ■ ■

25.41% 45 140 184 281 I i, 480 • ■ i • ' • • i ■ 11ITT • ' i ■ ■ ■ ■ i ' ' 1 ■ i ■ miz-> 50 100 150 200 250 300 350 400 450 500 Abundance #51296: Benzoic acid. 2.6-bis[(trimethylsilyl)oxy]-. trimet 73 355 __ - 22.40 22.60 22.80 23.00 23.20 5000 m/z 221.05 18.17% 147 267 47 208 237 ? m/z-> 50 100 150 200 250 300 350 400 450 ' 500 Abundance #58326: N-(Trifluoroacety!)-0,O ’,0"-tris(trimethylsilyl)no । • i • • • ■ i • ' ■ ‘ I • ■ 73 22.40 22.60 22.80 23.00 23.20 355 m/z 281.00 14.25% 5000 45 I 1, ' ‘ I ' 126147 • ‘i ■ • 193 265 1 ‘ ‘ I ' • 1 '■ I ' 1 1 1 I 1*t1}d/r 376 481 ' ' I ' 1 f ' I 1 i ■ ■ • ■ i • ■ miz-> 50 100 150 200 250 300 350 400 450 500 22.40 22.60 22.80 23.00 23.20

LBD.D GCMS1126.M Wed Jan 23 09:02:41 2002 Page 10

NYC-WTC_000018084

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NYC-WTC_000018084Source: NYC Law Department, mirrored locally

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