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GCMS blank analysis results

Machine-extracted title · confidence 95%

Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.

NYC-WTC_000017344–000017363

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document the LSC Area Percent Report ‘Data ‘File : C:\HPCHEM\1\DATA\JAN0802\LB.D Vial: 7 Acq On : 8 Jan 2002 7:12 pm Operator: 209 GALOS Sample : goms scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator! Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thre: 0.2 Max Peaks: 100 Stop Thre : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # = min scan scan scan TY height area % max. total 1 7.465 260 264 279 rBV 382028 1006385 11.63% 1.981% 2 11.523 701 706 726 rBV 2679763 6646795 76.79% 13.083% 3 14.167 985 994 1002 rvB 384171 745913 8.62% 1.468% 4 15.122 1093 1098 1117 rBV 3927941 8199590 94.73% 16.139% 5 17.306 1325 1336 1345 rBV 936495 1857461 21.468 3.656% 6 18.004 1407 1412 1418 rBV 115080 209639 2.42% 0.413% 7 20.125 1638 1643 1651 rBV 727957 1429771 16.52% 2.814% 8 20.391 1666 1672 1688 rBV 3995118 8490748 98.09% 16.712% 9 20.850 1717 1722 1733 rBV 389543 737123 8.52% 1.451% 10 22.640 1910 1917 1924 rBV 453588 901409 10.41% 1.774% 11 24.807 2147 2153 2166 rBV2 3901913 8655735 100.00% 17.037% 12 26.735 2357 2363 2370 rBV 184410 366510 4.23% 0.721% 13 28.497 2549 2555 2562 rBV 120494 254199 2.94% 0.500% 14 29.883 2701 2706 2714 rBV 491038 936641 10.82% 1.844% 15 30.095 2724 2729 2737 rVB 104707 215049 «2.48% 0.423% 16 31.563 2883 2889 2897 rBV 72480 166853 1.93% 0.328% 17 32.840 3021 3028 3035 rBV2 2346559 5470136 63.20% 10.767% 18 32.931 3035 3038 3049 rvB 86236 210099 2.43% 0.414% 19 34.217 3172 3178 3184 rBV2 46302 107823 1.25% 0.212% 20 35.410 3297 3308 3326 rBV2 104168 321390 3.71% 0.633% 21 36.906 3463 3471 3495 rBV2 1431463 3876659 44.79% 7.630% Sum of corrected areas: 50805928 LB.D GCMS0103.M Wed Jan 09 12:33:00 2002 NYC-WTC_000017348

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NYC-WTC_000017348Source: NYC Law Department, mirrored locally

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