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GCMS blank analysis results

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Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.

NYC-WTC_000017344–000017363

Folder label: “GCMS X 12/20/01 A 1/8/02

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NYC 9/11 Public Portal Document Alte Quantitation Report (QT Reviewed) , “4 "Datta File : C:\HPCHEM\1\DATA\JAN0802\LB.D Vial: 7 Acg On : 8 Jan 2002 7:12 pm Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 8 20:00 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update +: Mon Jan 07 10:31:02 2002 Response via : Initial Calibration DataAcg Meth : GCMS0103 Internal Standards R.T. QIon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.53 152 1054686 20.00 ug/l 0.00 10) Naphthalene-ds 15.12 136 3996564 20.00 ug/l 0.00 17) Acenaphthene-d10 20.39 164 1928394 20.00 ug/l 0.00 29) Phenanthrene-d10 24.81 188 2854444 20.00 ug/1 0.00 38) Chrysene-di2 32.84 240 1704327 20.00 ug/l 0.00 44) Perylene-di2 36.91 264 1035035 20.00 ug/1 0.01 System Monitoring Compounds 37) 2,4-DDD 29.88 235 149143 4.55 ug/mL -0.19 Spiked Amount 5.000 Recovery = 91.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.15 74 168 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 C) N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 13.40 77 172 N.D. 12) Isophorone 14.05 82 376 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0) N.D. 15) Naphthalene 15.18 128 1267 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 18.20 162 209 N.D. 20) Dimethylphthalate 19.81 163 291 N.D. 21) 2,6-Dinitrotoluene 20.12 165 355 N.D. 22) Acenaphthylene 20.07 152 338 N.D. 23) Acenaphthene 20.47 153 414 N.D. 24) 2,4-Dinitrotoluene 21.30 165 181 N.D. 25) Diethylphthalate 21.91 149 2208 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 ° N.D. 27) Fluorene 22.02 166 459 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 C) N.D. (#) = qualifier out of range (m) = manual integration LB.D GCMS1126.M Wed Jan 09 10:05:52 2002 Page 1 NYC-WTC_000017345

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NYC-WTC_000017345Source: NYC Law Department, mirrored locally

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