Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31250 using GCMS on February 11, 2002.
NYC-WTC_000016940–000016950Folder label: “GCMS X 12/24/01 A 1/10/02”
OCR status: ocr · source: ours
NYC 9/11 Public Portal Document oe Quantitation Report (QT Reviewed) . Data File : C:\HPCHEM\1\DATA\JANO902\31250.D Vial: 6 Acg On : 10 Jan 2002 8:25 pm Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Feb 5 16:25 2002 Quant Results File: GCMS0103.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update +: Thu Dec 13 14:40:46 2001 Response via : Initial Calibration DataAcg Meth : GCMS0103 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.53 152 645274 20.00 ug/1 0.00 10) Naphthalene-ds 15.12 136 2524548 20.00 ug/1 0.00 17) Acenaphthene-d10 20.39 164 1280472 20.00 ug/1 0.00 29) Phenanthrene-di0 24.80 188 1785563 20.00 ug/1 0.00 38) Chrysene-di2 32.84 240 1037135 20.00 ug/1 0.00 44) Perylene-d12 36.90 264 596600 20.00 ug/l 0.00 System Monitoring Compounds 37) 2,4-DDD 29.89 235 109902 5.36 ug/mL -0.18 Spiked Amount 5.000 Recovery = 107.20% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0) N.D. 3) bis(2-Chloroethyl) ether 0.00 93 0) N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 ° N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 ° N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 ) N.D. 12) Isophorone 0.00 82 Cy) N.D. 13) bis(2-Chloroethoxy) methane 0.00 93 ° N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.18 128 2148 N.D. 16) Hexachlorobutadiene 0.00 225 oO: N.D. 18) Hexachlorocyclopentadiene 0.00 237 ° N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 to) N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0) N.D. 23) Acenaphthene 0.00 153 ° N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 21.92 149 1083 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. (#) = qualifier out of range (m) = manual integration 31250.D GCMS0103.M Tue Feb 05 16:26:19 2002 Page 1 NYC-WTC_000016942
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NYC-WTC_000017004
Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31342 using GCMS on February 11, 2002.
Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016970
Laboratory report detailing GCMS analysis of sample AD31345 conducted on February 11, 2002.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017016
Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31346 using GCMS on February 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016951
Laboratory report detailing GCMS analysis of sample AD31277 conducted on February 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018994
Laboratory report documenting GCMS analysis of sample AD31133 performed on February 11, 2002, including detection of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017108
Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD30487 using GCMS on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016929
Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31249 using GCMS on February 11, 2002.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016992
Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31275 using GCMS on February 11, 2002.
Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019015
GCMS analysis report for sample AD31216 showing detection of unknown compounds and surrogate recovery data from February 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016981
Laboratory commentary noting the absence of unusual compounds in environmental sample AD31343 based on a GCMS scan from February 11, 2002.
Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016891
Laboratory GCMS analysis report for sample AD30110 conducted on January 9, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018238
Gas chromatography-mass spectrometry analysis of sample AD30983 performed on 1/25/02, detecting 2,4-DDD compound at 101 micrograms with 5.0 MDL.
Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000016908
Fragmented DEP GCMS record from late December 2001 to mid-January 2002 with no readable text.
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NYC-WTC_000016909
DEP GCMS method documentation page including data tables and extraction parameters for environmental analysis.
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NYC-WTC_000016912
Laboratory calibration report from the DEP testing for volatile organic compounds using GCMS analysis on January 10, 2002.
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NYC-WTC_000016916
Reference data sheet from the DEP laboratory documenting GCMS analysis parameters and results for volatile organic compounds.
Filed in the same folder
NYC-WTC_000016921
Laboratory report documenting a GCMS blank analysis for sample AD31249 conducted on January 29, 2002.
Filed in the same folder