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GCMS analysis log for sample AD30608

Machine-extracted title · confidence 95%

Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD30608 performed on January 22, 2002.

NYC-WTC_000017192–000017209

Folder label: “GCMS X 12/17/01 A 12/28/01 1/3/01 1/4/01

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NYC 9/11 Public Portal Document ae Quantitation Report (QT Reviewed) * .. Data File : C:\HPCHEM\1\DATA\DEC2701\30608.D Vial: 32 Acq On : 28 Dec 2001 8:16 pm Operator: 209 GALOS sample : GC/MS SCAN 12/17 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 31 14:10 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcg Meth : GCMS1126 Internal Standards R.T. QIon Response Conc Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.68 152 1021716 20.00 ug/l -0.02 10) Naphthalene-ds 15.28 136 3965981 20.00 ug/l ~-0.02 17) Acenaphthene-d10 20.56 164 1978494 20.00 ug/l = -0.01 29) Phenanthrene-di0 24.99 188 2901181m 20.00 ug/l 0.00 38) Chrysene-d12 33.02 240 1801278 20.00 ug/l -0.01 44) Perylene-d12 37.11 264 1090104 20.00 ug/l 0.00 System Monitoring Compounds 37) 2,4-DDD 30.06 235 143965 4.51 ug/ml 0.00 Spiked Amount 5.000 Recovery = 90.20% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.17 74 1585 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 ° N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0) N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 ° N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 oO N.D. 11) Nitrobenzene 12.94 77 205 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 ° N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 1552 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0) N.D. 19) 2-Chloronaphthalene 0.00 162 0) N.D. . 20) Dimethylphthalate 20.28 163 324 N.D. 21) 2,6-Dinitrotoluene 0.00 165 ° N.D. 22) Acenaphthylene 0.00 152 ° N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.24 165 182 N.D. 25) Diethylphthalate 22.12 149 901 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0) N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. (#) = qualifier out of range (m) = manual integration 30608.D GCMS1126.M Mon Dec 31 14:10:51 2001 Page 1 NYC-WTC_000017194

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