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← Document results/DEP Box 22/GCMS X 11/29/01 A 12/7/01
Document / 11 pages

GCMS analysis comments, sample AD28971, Dec 2001

Machine-extracted title · confidence 90%

Lab report noting no unusual compounds but recovery issues in a water sample.

NYC-WTC_000035629–000035639

Folder label: “GCMS X 11/29/01 A 12/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC0 701\28971.D Vial: 16 Acq On 8 Dec 2001 5:34 am Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 14:52 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.68 152 882413 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3364730 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1691126 20.00 ug/1 -0.02 2 9) Phenanthrene-dl0 24.98 188 2451686 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 1692618 20.00 ug/1 -0.02 44) Perylene-dl2 37.11 264 1164932 20.00 ug/1 -0.01

System Monitoring Compounds 37) 2,4-DDD 30.06 235 159336 5.46/ug/mL -0.01 Spiked Amount 5.000 Recovery = 109.20 Target Compounds alue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 12.96 77 355 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 813 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Ac enaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.10 165 365 N.D. 25) Diethylphthalate 22.08 149 1036 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 23.08 77 311 N.D.

(#) = qualifier out of range (m) = manual integration 28971.D GCMS1126.M Thu Dec 13 15:39:24 2001 Page 1

NYC-WTC_000035631

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NYC-WTC_000035631Source: NYC Law Department, mirrored locally

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