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GCMS analysis comments, sample AD28903, Dec 2001

Machine-extracted title · confidence 95%

GCMS scan results for sample AD28903 dated December 15, 2001, detecting bis(2-Ethylhexyl)phthalate.

NYC-WTC_000035580–000035588

Folder label: “GCMS X 11/29/01 A 12/7/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\DEC0 701\28903.D Vial: 9 Acq On 7 Dec 2001 10:44 pm Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 14:52 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 850514 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3260335 20.00 ug/1 -0.03 17) Acenaphthene-dl0 20.55 164 1646099 20.00 ug/1 -0.02 2 9) Phenanthrene -dl0 24.98 188 2368831 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1522586 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 1095222 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.05 235 150913 5. ug/mL .02 Spiked Amount 5.000 Recovery 107.00%

Target Compounds alue 2) N-nitroso-dimethyl amine 5.17 74 1198 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 1420 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.08 165 188 N.D. 25) Diethylphthalate 22.08 149 1461 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 23.08 77 109 N.D.

(#) = qualifier out of range (m) = manual integration 28903.D GCMS1126.M Thu Dec 13 14:55:54 2001 Page 1

NYC-WTC_000035582

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NYC-WTC_000035582Source: NYC Law Department, mirrored locally

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