NYC-WTC_000035651
Lab report noting bis(2-Ethylhexyl)phthalate detection and recovery issues in a water sample.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 11 pages
GCMS analysis comments, sample AD28969, Dec 2001
Machine-extracted title · confidence 90%Lab report noting bis(2-Ethylhexyl)phthalate detection and recovery issues in a water sample.
NYC-WTC_000035618–000035628Folder label: “GCMS X 11/29/01 A 12/7/01”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\HPCHEM\l\DATA\DEC0701\28969.D Vial: 14 Acq On 8 Dec 2001 3:37 am Operator: 209 GALOS Sample 11/29 gc/ms scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 12 14:51 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Nov 28 15:06:24 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.67 152 845969 20.00 ug/1 -0.02 10) Naphthalene-d8 15.27 136 3240298 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.55 164 1642541 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98- 188 2338941 20.00 ug/1 -0.01 38) Chrysene-dl2 33.01 240 1468338 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 845848 20.00 ug/1 -0.01
System Monitoring Compounds 37) 2,4-DDD 30.05 235 161579 5/80 ug/mL 0.02 Spiked Amount 5.000 Recovery = 116.00%
Target Compounds alue 2) N-nitroso-dimethyl amine 5.13 74 110 N.D.-- 3) bis(2-Chloroethyl )ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 13.57 82 183 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 844 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.02 165 264 N.D. 25) Diethylphthalate 22.08 149 1078 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 28969.D GCMS1126.M Thu Dec 13 15:37:27 2001 Page 1
NYC-WTC_000035620
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Laboratory analysis report for sample AD29296 conducted on December 28, 2001, including surrogate recovery data.
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Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036469
Laboratory report documenting GCMS analysis of sample AD29461 conducted on January 4, 2002, showing unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000035820
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1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Filed elsewhere
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