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GCMS unknowns analysis report for sample AD30423, Jan 2002

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Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD30423 using GCMS on January 18, 2002.

NYC-WTC_000017088–000017096

Folder label: “GCMS X 12/14/01 A 1/1/02

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NYC 9/11 Public Portal Document i 7 Quantitation Report (QT Reviewed) . Data File : C:\HPCHEM\1\DATA\DEC3101\30423.D Vial: 24 Acq On : 1 Jan 2002 9:17 am Operator: 209 GALOS Sample : gems scan 12/1l4a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 1 10:06 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126 Internal Standards R.T. QIon Response Conc Units Dev (Min) 1) 1,4-Dichlorobenzene-d4 11.68 152 822232 20.00 ug/l -0.02 10) Naphthalene-ds 15.28 136 3175236 20.00 ug/l -0.03 17) Acenaphthene-d10 20.57 164 1631653 20.00 ug/l -0.01 29) Phenanthrene-d10 24,98 188 2302662 20.00 ug/l -0.01 38) Chrysene-di2 33.02 240 1368813 20.00 ug/l = -0.01 44) Perylene-di2 37.12 264 751011 20.00 ug/1 0.00 System Monitoring Compounds 37) 2,4-DDD 30.07 235 142838 5.64 ug/ml 0.00 Spiked Amount 5.000 Recovery = 112.80% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis (2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0) N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 ° N.D. 9) Hexachloroethane 0.00 117 ° N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 C) N.D. 15) Naphthalene 15.33 128 964 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 ° N.D. 19) 2-Chloronaphthalene 0.00 162 ° N.D. 20) Dimethylphthalate 0.00 163 0) N.D. 21) 2,6-Dinitrotoluene 0.00 165 ° N.D. 22) Acenaphthylene 0.00 152 0 N.D. * 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.30 165 178 N.D. 25) Diethylphthalate 22.15 149 446 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0) N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. (#) = qualifier out of range (m) = manual integration 30423.D GCMS0103.M Tue Jan 15 14:40:36 2002 Page 1 NYC-WTC_000017090

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NYC-WTC_000017090Source: NYC Law Department, mirrored locally

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