GCMS analysis report for sample AD30111, January 2002

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Laboratory GCMS analysis report for sample AD30111 conducted on January 9, 2002, by analyst DLV.

NYC-WTC_000016826–000016834

Folder label: “GCMS X 12/12/01 A 12/20/01”

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NYC 9/11 Public Portal Document : 7 Quantitation Report (QT Reviewed) . Data File : C:\HPCHEM\1\DATA\JANO302\30111.D Vial: 34 Acq On : 4 Jan 2002 6:41 pm Operator: 209 GALOS Sample : gems scan 1/2a Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 4 19:29 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126 Internal Standards R.T. Qlon Response Conc Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.52 152 733410 20.00 ug/l -0.17 10) Naphthalene-ds 15.12 136 2860781 20.00 ug/l -0.18 17) Acenaphthene-d10 20.39 164 1440494 20.00 ug/l -0.18 29) Phenanthrene-d10 24.81 188 2026552 20.00 ug/l -0.18 38) Chrysene-d12 32.83 240 1170282 20.00 ug/l = -0.20 44) Perylene-d12 36.90 264 642813 20.00 ug/l -0.22 System Monitoring Compounds 37) 2,4-DDD 29.88 235 125766 5.64 ug/mL -0.19 Spiked Amount 5.000 Recovery = 112.80% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 ° N.D. 3) bis (2-Chloroethyl) ether 0.00 93 fe) N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 Ce) N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0) N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 ° N.D. 9) Hexachloroethane 0.00 117 C) N.D. 11) Nitrobenzene 0.00 77 ) N.D. 12) Isophorone 0.00 82 ) N.D. 13) bis (2-Chloroethoxy) methane 0.00 93 ) N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 ° N.D. 15) Naphthalene 15.18 128 1001 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 CO) N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 ° N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0) N.D. 23) Acenaphthene 0.00 153 0) N.D. 24) 2,4-Dinitrotoluene 20.73 165 285 N.D. 25) Diethylphthalate 21.93 149 564 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 () N.D. 27) Fluorene 0.00 166 C) N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 [) N.D. (#) = qualifier out of range (m) = manual integration 30111.D GCMS0103.M Mon Jan 07 11:35:42 2002 Page 1 NYC-WTC_000016828

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NYC-WTC_000016828Source: NYC Law Department, mirrored locally

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