GCMS analysis report for sample AD30117, January 2002

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) ° . ‘Data File : C:\HPCHEM\1\DATA\JAN0302\30117.D Vial: 10 Acq On : 3 Jan 2002 7:21 pm Operator: 209 GALOS Sample : gems scan 12/12 Inst. : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 3 20:10 2002 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update -: Fri Dec 28 15:11:00 2001 Response via : Initial Calibration DataAcg Meth : GCMS1126 Internal Standards R.T. Qlon Response Conc Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.53 152 1142039 20.00 ug/l -0.17 10) Naphthalene-ds 15.13 136 4374308 20.00 ug/l -0.18 17) Acenaphthene-d10 20.40 164 2155738 20.00 ug/l -0.18 29) Phenanthrene-d10 24.81 188 3230963 20.00 ug/l -0.18 38) Chrysene-di2 32.84 240 1914883 20.00 ug/l -0.20 44) Perylene-d12 36.91 264 1107318 20.00 ug/l = -0.21 System Monitoring Compounds 37) 2,4-DDD 29.89 235 168770 4.75 ug/mL -0.18 Spiked Amount 5.000 Recovery = 95.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.15 74 454 N.D. 3) bis(2-Chloroethyl) ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0) N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. + 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 12.89 77 199 N.D. 12) Isophorone 0.00 82 C) N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 ° N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0) N.D. 15) Naphthalene 15.17 128 2515 N.D. 16) Hexachlorobutadiene 0.00 225 ° N.D. 18) Hexachlorocyclopentadiene 0.00 237 Co) N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0) N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 ° N.D. 24) 2,4-Dinitrotoluene 21.09 165 196 N.D. 7 25) Diethylphthalate 21.92 149 1035 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 ° N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0) N.D. (#) = qualifier out of range (m) = manual integration 30117.D GCMSO103.M Mon Jan 07 10:32:43 2002 Page 1 NYC-WTC_000016775