GCMS analysis results for sample AD29733, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD29733 conducted on January 9, 2002, by the DEP.

NYC-WTC_000037177–000037187

Folder label: “GCMS X 12/10/01 A 12/15/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1401\29733.D Vial: 20 Acq On : 15 Dec 2001 9:03 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 15 21:52 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.67 152 911681 20.00 ug/1 -0.03 10) Naphthalene-d8 15.28 136 3500129 20.00 ug/1 -0.03 17) Acenaphthene-dlO 20.56 164 1787172 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.97 188 2581060 20.00 ug/1 -0.02 38) Chrysene-dl2 33.01 240 1649057 20.00 ug/1 -0.02 44) Perylene-dl2 37.10 264 1008402 20.00 ug/1 -0.02

System Monitoring Compounds 37) 2,4-DDD 30.05 235 145212 3.89 ug/mL -0.02 Spiked Amount 5.000 Recovery = 77.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl )ether 11.01 93 637 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,21 -oxybis(l-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 14.04 82 13497 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.34 128 814 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.00 163 7517 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 20.64 153 323 N.D. 24) 2,4-Dinitrotoluene 21.46 165 231 N.D. 25) Diethylphthalate 22.07 149 41047 0.37 ug/1 97 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 22.20 166 1551 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 29733.D GCMS1126.M Fri Dec 28 12:52:55 2001 Page 1

NYC-WTC_000037179

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