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GCMS analysis results for sample AD29733, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD29733 conducted on January 9, 2002, by the DEP.

NYC-WTC_000037177–000037187

Folder label: “GCMS X 12/10/01 A 12/15/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1401\29733.D Vial: 20 • Acq On : 15 Dec 2001 9:03 pm Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 15 21:52 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 22.65 168 1165 N.D. 31) 4-Bromophenyl-phenylether 23.68 248 107 N.D. 32) Hexachlorobenzene 24.09 284 750 N.D. 33) Phenanthrene 25.04 178 8119 N.D. 34) Anthracene 25.18 178 9771 N.D. 35) Di-n-butylphthalate 26.99 149 44320 N.D. 36) Fluoranthene 28.68 202 9435 N.D. 39) Pyrene 29.34 202 9762 N.D. 40) Butylbenzylphthalate 31.50 149 562 N.D. 41) Benzo(a)anthracene 33.01 228 6084 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 8890 • N.D. 43) Chrysene 33.10 228 2239 N.D. 45) Di-n-Octylphthalate 35.03 149 671 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.10 252 4102 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 29733.D GCMS1126.M Fri Dec 28 12:52:59 2001 Page 2

NYC-WTC_000037180

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NYC-WTC_000037180Source: NYC Law Department, mirrored locally

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